2-phenylethenyl(triphenylphosphine)gold(I)

Base Information

Chemical Name:2-phenylethenyl(triphenylphosphine)gold(I)
CAS No.:57947-31-6
Molecular Formula:C₂₆H₂₂AuP
Molecular Weight:562.401
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-phenylethenyl(triphenylphosphine)gold(I)

Chemical Property:

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Technology Process of 2-phenylethenyl(triphenylphosphine)gold(I)

There total 1 articles about 2-phenylethenyl(triphenylphosphine)gold(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 14243-64-2
(triphenylphosphine)gold(I) chloride

: 57947-31-6,57947-32-7
2-phenylethenyl(triphenylphosphine)gold(I)

Guidance literature:: In tetrahydrofuran; (Ar); addn. of THF soln. of 2-phenylethenylmetalloderiv. to THF soln. ofgold compd. at -20°C, stirring for 20 min, warming to room temp. , stirring for 1 h; A.S.K. Hashmi, T.D. Ramamurthi and F. Rominger, J. Organomet. Chem., 2009, 694, 592; evapn. in vac., addn. of benzene, filtration through celite, evapn. in vac., washing with pentane, drying, extn. (benzene), filtration, washing with pentane, drying in high vac., NMR and MS;
DOI:10.1039/c2ob06788a

Reference yield:

: 57947-31-6,57947-32-7
2-phenylethenyl(triphenylphosphine)gold(I)

: 3058-39-7
4-iodobenzonitrile

: 21209-78-9,79384-12-6
iodo(triphenylphosphine)gold(I)

Guidance literature:: With PdCl₂(dppf) (1 molpercent); In acetonitrile; byproducts: NCC6H4CHCHC6H5; 24 h;
DOI:10.1002/anie.200902942

Reference yield:

: 57947-31-6,57947-32-7
2-phenylethenyl(triphenylphosphine)gold(I)

: 4392-24-9
Cinnamyl bromide

: 26057-47-6,26057-48-7,52267-15-9,26057-49-8
(1E,4Z)-1,5-diphenyl-1,4-pentadiene

: 26057-47-6,26057-49-8,52267-15-9,26057-48-7
(E,E)-1,5-diphenyl-1,4-pentadiene

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; at 80 ℃; optical yield given as %de; regioselective reaction; Inert atmosphere;
DOI:10.1039/c2ob06788a