Technology Process of C17H17NO5S
There total 3 articles about C17H17NO5S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: diethyl ether; water / 6 h / 20 °C
2: potassium carbonate / acetonitrile
3: carbon dioxide / N,N-dimethyl acetamide / 10 h / 20 °C / 760.05 Torr / Schlenk technique; Irradiation
4: caesium carbonate / N,N-dimethyl acetamide / 10 h / 60 °C / Schlenk technique
With
carbon dioxide; potassium carbonate; caesium carbonate;
In
diethyl ether; N,N-dimethyl acetamide; water; acetonitrile;
DOI:10.1002/anie.201206166
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / acetonitrile
2: carbon dioxide / N,N-dimethyl acetamide / 10 h / 20 °C / 760.05 Torr / Schlenk technique; Irradiation
3: caesium carbonate / N,N-dimethyl acetamide / 10 h / 60 °C / Schlenk technique
With
carbon dioxide; potassium carbonate; caesium carbonate;
In
N,N-dimethyl acetamide; acetonitrile;
DOI:10.1002/anie.201206166
- Guidance literature:
-
Multi-step reaction with 2 steps
1: carbon dioxide / N,N-dimethyl acetamide / 10 h / 20 °C / 760.05 Torr / Schlenk technique; Irradiation
2: caesium carbonate / N,N-dimethyl acetamide / 10 h / 60 °C / Schlenk technique
With
carbon dioxide; caesium carbonate;
In
N,N-dimethyl acetamide;
DOI:10.1002/anie.201206166
