[2-(phenylazo)phenyl-C,N']tellurenyl iodide

Base Information

Chemical Name:[2-(phenylazo)phenyl-C,N']tellurenyl iodide
CAS No.:203128-22-7
Molecular Formula:C₁₂H₉IN₂Te
Molecular Weight:435.721
Hs Code.:

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Chemical Property of [2-(phenylazo)phenyl-C,N']tellurenyl iodide

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Technology Process of [2-(phenylazo)phenyl-C,N']tellurenyl iodide

There total 2 articles about [2-(phenylazo)phenyl-C,N']tellurenyl iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: 51343-11-4
1-(2-iodophenyl)-2-phenyldiazene

: 203128-22-7
[2-(phenylazo)phenyl-C,N']tellurenyl iodide

: bis[2-(phenylazo)phenyl-C,N']telluride

Guidance literature:: 1-(2-iodophenyl)-2-phenyldiazene; With n-butyllithium; In diethyl ether; at -114 ℃; for 0.5h; Inert atmosphere;

With tellurium(II) iodide; In diethyl ether; at -114 - 20 ℃; Inert atmosphere;
DOI:10.1021/om1009022

Reference yield:

: [2-(phenylazo)phenyl-C,N']mercury(II) chloride

: 203128-22-7
[2-(phenylazo)phenyl-C,N']tellurenyl iodide

: bis[2-(phenylazo)phenyl-C,N']telluride

Guidance literature:: Multi-step reaction with 2 steps

1.1: iodine / chloroform / 18 h / 20 °C / Inert atmosphere

2.1: n-butyllithium / diethyl ether / 0.5 h / -114 °C / Inert atmosphere

2.2: -114 - 20 °C / Inert atmosphere

With n-butyllithium; iodine; In diethyl ether; chloroform;
DOI:10.1021/om1009022