C₁₅H₁₂N₂O₂S

Base Information

• Chemical Name: C₁₅H₁₂N₂O₂S
• CAS No.: 1297474-46-4
• Molecular Formula: C₁₅H₁₂N₂O₂S
• Molecular Weight: 284.338
• Mol file: 1297474-46-4.mol

Synonyms:

Chemical Property of C₁₅H₁₂N₂O₂S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₅H₁₂N₂O₂S

There total 2 articles about C₁₅H₁₂N₂O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C15H16N2O2S (1297474-37-3) → C15H12N2O2S (1297474-46-4)

Guidance literature:

With chloranil; In 1,4-dioxane; at 90 ℃; for 5h;

DOI:10.1016/j.tetlet.2010.12.081

Reference yield:

4-(4-hydroxyphenyl)cyclohexan-1-one (105640-07-1) → C15H12N2O2S (1297474-46-4)

Guidance literature:

Multi-step reaction with 2 steps

1: piperidine; sulfur / ethanol / 4 h / 50 °C

2: chloranil / 1,4-dioxane / 5 h / 90 °C

With piperidine; chloranil; sulfur; In 1,4-dioxane; ethanol; 1: Gewald reaction;

DOI:10.1016/j.tetlet.2010.12.081

Reference yield:

C15H12N2O2S (1297474-46-4) → C25H18N2O6S (1297474-22-6)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrogenchloride / butan-1-ol / 2 h / Reflux

2: water; sodium hydroxide / ethanol / 2 h / Reflux

With hydrogenchloride; water; sodium hydroxide; In ethanol; butan-1-ol;

DOI:10.1016/j.tetlet.2010.12.081

upstream raw materials:

C₁₅H₁₆N₂O₂S

4-(4-hydroxyphenyl)cyclohexan-1-one

Downstream raw materials:

C₂₅H₁₈N₂O₆S

C₂₇H₂₂N₂O₆S

Refernces