allyl 3-[dimethyl(thexyl)silyloxy]-{(R)-2-[2-(2-hydroxyethoxy)acetylamino]-2-methoxycarbonylethylsulfanylmethyl}-5-methoxy-6-methylbenzoate

Base Information

Chemical Name:allyl 3-[dimethyl(thexyl)silyloxy]-{(R)-2-[2-(2-hydroxyethoxy)acetylamino]-2-methoxycarbonylethylsulfanylmethyl}-5-methoxy-6-methylbenzoate
CAS No.:1275616-74-4
Molecular Formula:C₂₉H₄₇NO₉SSi
Molecular Weight:613.845
Hs Code.:

allyl 3-[dimethyl(thexyl)silyloxy]-{(R)-2-[2-(2-hydroxyethoxy)acetylamino]-2-methoxycarbonylethylsulfanylmethyl}-5-methoxy-6-methylbenzoate

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Chemical Property of allyl 3-[dimethyl(thexyl)silyloxy]-{(R)-2-[2-(2-hydroxyethoxy)acetylamino]-2-methoxycarbonylethylsulfanylmethyl}-5-methoxy-6-methylbenzoate

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Technology Process of allyl 3-[dimethyl(thexyl)silyloxy]-{(R)-2-[2-(2-hydroxyethoxy)acetylamino]-2-methoxycarbonylethylsulfanylmethyl}-5-methoxy-6-methylbenzoate

There total 2 articles about allyl 3-[dimethyl(thexyl)silyloxy]-{(R)-2-[2-(2-hydroxyethoxy)acetylamino]-2-methoxycarbonylethylsulfanylmethyl}-5-methoxy-6-methylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₈H₆₁NO₉SSi

: 1275616-74-4
allyl 3-[dimethyl(thexyl)silyloxy]-{(R)-2-[2-(2-hydroxyethoxy)acetylamino]-2-methoxycarbonylethylsulfanylmethyl}-5-methoxy-6-methylbenzoate

Guidance literature:: With toluene-4-sulfonic acid; In methanol; at 60 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/jm1014023

Reference yield:

: 676347-22-1
allyl (R)-2-[2-amino-2-(methoxycarbonyl)ethylsulfanylmethyl]-3-[dimethyl(thexyl)silyloxy]-5-methoxy-6-methylbenzoate

: 1275616-74-4
allyl 3-[dimethyl(thexyl)silyloxy]-{(R)-2-[2-(2-hydroxyethoxy)acetylamino]-2-methoxycarbonylethylsulfanylmethyl}-5-methoxy-6-methylbenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1,2-dichloro-ethane / acetonitrile / 5 h / 0 °C / Inert atmosphere

2: toluene-4-sulfonic acid / methanol / 0.5 h / 60 °C / Inert atmosphere

With toluene-4-sulfonic acid; 1,2-dichloro-ethane; In methanol; acetonitrile;
DOI:10.1021/jm1014023

Reference yield:

: 1275616-74-4
allyl 3-[dimethyl(thexyl)silyloxy]-{(R)-2-[2-(2-hydroxyethoxy)acetylamino]-2-methoxycarbonylethylsulfanylmethyl}-5-methoxy-6-methylbenzoate

: C₂₆H₄₃NO₉SSi

Guidance literature:: With morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 0 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jm1014023