Technology Process of C29H24F6N2S2
There total 4 articles about C29H24F6N2S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C39H40F6N2O4S2;
With
trifluoroacetic acid;
In
dichloromethane;
at 20 ℃;
for 2h;
With
sodium hydrogencarbonate;
In
dichloromethane; water;
DOI:10.1002/anie.201304301
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / tetrahydrofuran / 24 h / Inert atmosphere; Reflux
2: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / water; 1,2-dimethoxyethane / 24 h / Inert atmosphere; Reflux
3: trifluoroacetic acid / dichloromethane / 2 h / 20 °C
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium(0); potassium acetate; sodium carbonate; trifluoroacetic acid;
In
tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water;
DOI:10.1002/anie.201304301
- Guidance literature:
-
Multi-step reaction with 3 steps
1: Iodine monochloride / dichloromethane / 2 h / 0 °C
2: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / water; 1,2-dimethoxyethane / 24 h / Inert atmosphere; Reflux
3: trifluoroacetic acid / dichloromethane / 2 h / 20 °C
With
tetrakis(triphenylphosphine) palladium(0); Iodine monochloride; sodium carbonate; trifluoroacetic acid;
In
1,2-dimethoxyethane; dichloromethane; water;
DOI:10.1002/anie.201304301
