C₁₇H₁₂BrN₃O

Base Information

• Chemical Name: C₁₇H₁₂BrN₃O
• CAS No.: 1610051-91-6
• Molecular Formula: C₁₇H₁₂BrN₃O
• Molecular Weight: 354.206
• Mol file: 1610051-91-6.mol

Synonyms:

Chemical Property of C₁₇H₁₂BrN₃O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₇H₁₂BrN₃O

There total 2 articles about C₁₇H₁₂BrN₃O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-amino-4-bromobenzoic acid (20776-50-5) → C17H12BrN3O (1610051-91-6)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium nitrite; hydrogenchloride; tin(ll) chloride / 2 h / -5 - 20 °C

2: acetic acid / 0.08 h / 150 °C / Microwave irradiation

With hydrogenchloride; acetic acid; tin(ll) chloride; sodium nitrite;

DOI:10.1016/j.bmcl.2014.04.051

Reference yield:

4-bromo-2-hydrazineylbenzoic acid + (3-methylbenzoyl)acetonitrile (53882-81-8) → C17H12BrN3O (1610051-91-6)

Guidance literature:

With acetic acid; at 150 ℃; for 0.0833333h; Microwave irradiation;

DOI:10.1016/j.bmcl.2014.04.051

Reference yield:

C17H12BrN3O (1610051-91-6) + phenylboronic acid (98-80-6) → C23H17N3O (1610051-70-1)

Guidance literature:

With potassium phosphate; palladium bis[bis(diphenylphosphino)ferrocene] dichloride; In 1,4-dioxane; water; at 130 ℃; for 0.666667h; Microwave irradiation;

DOI:10.1016/j.bmcl.2014.04.051 DOI:10.1016/j.bmcl.2014.04.051

upstream raw materials:

(3-methylbenzoyl)acetonitrile

2-amino-4-bromobenzoic acid

Downstream raw materials:

C₂₃H₁₇N₃O

C₂₄H₁₉N₃O₂

C₂₂H₁₆N₄O

C₂₄H₁₉N₃O