Boc-L-(?-Me)-His-AGly-L-Cha-L-Phe-βAsp-(OBzl)2

Base Information

Chemical Name:Boc-L-(?-Me)-His-AGly-L-Cha-L-Phe-βAsp-(OBzl)2
CAS No.:1360187-66-1
Molecular Formula:C₆₀H₇₇N₇O₁₀
Molecular Weight:1056.31
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Boc-L-(?-Me)-His-AGly-L-Cha-L-Phe-βAsp-(OBzl)2

Chemical Property:

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Technology Process of Boc-L-(?-Me)-His-AGly-L-Cha-L-Phe-βAsp-(OBzl)2

There total 10 articles about Boc-L-(?-Me)-His-AGly-L-Cha-L-Phe-βAsp-(OBzl)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₂H₅₃N₃O₈

: 1360187-66-1
Boc-L-(?-Me)-His-AGly-L-Cha-L-Phe-βAsp-(OBzl)2

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride / 1,4-dioxane / 0.5 h

2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane

3: hydrogenchloride / 1,4-dioxane / 0.5 h

4: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane

With hydrogenchloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In 1,4-dioxane; dichloromethane;
DOI:10.1039/c2cc17435a

Reference yield:

: C₃₃H₃₈N₂O₇

: 1360187-66-1
Boc-L-(?-Me)-His-AGly-L-Cha-L-Phe-βAsp-(OBzl)2

Guidance literature:: Multi-step reaction with 6 steps

1: hydrogenchloride / 1,4-dioxane / 0.5 h

2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane

3: hydrogenchloride / 1,4-dioxane / 0.5 h

4: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane

5: hydrogenchloride / 1,4-dioxane / 0.5 h

6: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane

With hydrogenchloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In 1,4-dioxane; dichloromethane;
DOI:10.1039/c2cc17435a

Reference yield:

: C₃₇H₄₅N₃O₆

: 1360187-66-1
Boc-L-(?-Me)-His-AGly-L-Cha-L-Phe-βAsp-(OBzl)2

Guidance literature:: Multi-step reaction with 3 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane

2: hydrogenchloride / 1,4-dioxane / 0.5 h

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane

With hydrogenchloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In 1,4-dioxane; dichloromethane;
DOI:10.1039/c2cc17435a