C₁₄H₁₈N₄O₂S

Base Information

Chemical Name:C₁₄H₁₈N₄O₂S
CAS No.:1618698-65-9
Molecular Formula:C₁₄H₁₈N₄O₂S
Molecular Weight:306.389
Hs Code.:

C<sub>14</sub>H<sub>18</sub>N<sub>4</sub>O<sub>2</sub>S

Synonyms:

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Chemical Property of C₁₄H₁₈N₄O₂S

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Technology Process of C₁₄H₁₈N₄O₂S

There total 9 articles about C₁₄H₁₈N₄O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1618698-46-6
(3R,4S,5S)-5-[(O-tert-butyldiphenylsilyl)hydroxymethyl]-3,4-isopropylidene-2-methyl-1-pyrroline-3,4-diol

: 1618698-65-9
C₁₄H₁₈N₄O₂S

Guidance literature:: Multi-step reaction with 7 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C

2: hydrogen; palladium 10% on activated carbon / methanol / 24 h / 10343.2 Torr

3: methanol / 6 h / 20 °C

4: Dess-Martin periodane / dichloromethane / 2 h / 20 °C

5: potassium carbonate; dimethyl 1-(1-diazo-2-oxopropyl)phosphonate / methanol / 7 h / 0 - 20 °C

6: trifluoroacetic acid / water / 2.5 h / 20 °C

7: copper(II) sulfate; sodium L-ascorbate / water; tert-butyl alcohol

With palladium 10% on activated carbon; tetrabutyl ammonium fluoride; hydrogen; dimethyl 1-(1-diazo-2-oxopropyl)phosphonate; potassium carbonate; Dess-Martin periodane; copper(II) sulfate; sodium L-ascorbate; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; water; tert-butyl alcohol; 4: |Dess-Martin Oxidation;
DOI:10.1039/c4ob00931b

Reference yield:

: 1449248-48-9
(2R,3S,4R,5S)-N-tert-butoxycarbonyl-2-formyl-3,4-O-isopropylidene-5-methylpyrrolidine-3,4-diol

: 1618698-65-9
C₁₄H₁₈N₄O₂S

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate; dimethyl 1-(1-diazo-2-oxopropyl)phosphonate / methanol / 7 h / 0 - 20 °C

2: trifluoroacetic acid / water / 2.5 h / 20 °C

3: copper(II) sulfate; sodium L-ascorbate / water; tert-butyl alcohol

With dimethyl 1-(1-diazo-2-oxopropyl)phosphonate; potassium carbonate; copper(II) sulfate; sodium L-ascorbate; trifluoroacetic acid; In methanol; water; tert-butyl alcohol;
DOI:10.1039/c4ob00931b

Reference yield:

: 1618698-48-8
(2S,3S,4R,5S)-2-hydroxymethyl-3,4-O-isopropylidene-5-methylpyrrolidine-3,4-diol

: 1618698-65-9
C₁₄H₁₈N₄O₂S

Guidance literature:: Multi-step reaction with 5 steps

1: methanol / 6 h / 20 °C

2: Dess-Martin periodane / dichloromethane / 2 h / 20 °C

3: potassium carbonate; dimethyl 1-(1-diazo-2-oxopropyl)phosphonate / methanol / 7 h / 0 - 20 °C

4: trifluoroacetic acid / water / 2.5 h / 20 °C

5: copper(II) sulfate; sodium L-ascorbate / water; tert-butyl alcohol

With dimethyl 1-(1-diazo-2-oxopropyl)phosphonate; potassium carbonate; Dess-Martin periodane; copper(II) sulfate; sodium L-ascorbate; trifluoroacetic acid; In methanol; dichloromethane; water; tert-butyl alcohol; 2: |Dess-Martin Oxidation;
DOI:10.1039/c4ob00931b