C₄₄H₄₈N₄O₉

Base Information

Chemical Name:C₄₄H₄₈N₄O₉
CAS No.:1373502-14-7
Molecular Formula:C₄₄H₄₈N₄O₉
Molecular Weight:776.887
Hs Code.:

C<sub>44</sub>H<sub>48</sub>N<sub>4</sub>O<sub>9</sub>

Synonyms:

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Chemical Property of C₄₄H₄₈N₄O₉

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Technology Process of C₄₄H₄₈N₄O₉

There total 13 articles about C₄₄H₄₈N₄O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2079-53-0
1-(4-(allyloxy)phenyl)ethanone

: 1373502-14-7
C₄₄H₄₈N₄O₉

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium methylate / methanol / 24 h / Reflux; Inert atmosphere

2.1: hydroxylamine monohydrate; toluene-4-sulfonic acid / methanol / 24 h / Reflux

3.1: lithium hydroxide / methanol; water / 2 h / Cooling with ice

4.1: pyridine; trichlorophosphate / chloroform / 1 h / Inert atmosphere

5.1: ozone / dichloromethane / -78 °C

6.1: methanol; N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

6.2: 9 h / 20 °C / Inert atmosphere

7.1: trifluoroacetic acid / dichloromethane / 2 h / Inert atmosphere

With pyridine; hydroxylamine monohydrate; sodium methylate; toluene-4-sulfonic acid; ozone; trifluoroacetic acid; lithium hydroxide; trichlorophosphate; In methanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; 6.1: Ugi reaction / 6.2: Ugi reaction;
DOI:10.1039/c2cc31294h

Reference yield:

: 1373502-18-1
methyl 5-(4-(allyloxy)phenyl)isoxazole-3-carboxylate

: 1373502-14-7
C₄₄H₄₈N₄O₉

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium hydroxide / methanol; water / 2 h / Cooling with ice

2.1: pyridine; trichlorophosphate / chloroform / 1 h / Inert atmosphere

3.1: ozone / dichloromethane / -78 °C

4.1: methanol; N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

4.2: 9 h / 20 °C / Inert atmosphere

5.1: trifluoroacetic acid / dichloromethane / 2 h / Inert atmosphere

With pyridine; ozone; trifluoroacetic acid; lithium hydroxide; trichlorophosphate; In methanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; 4.1: Ugi reaction / 4.2: Ugi reaction;
DOI:10.1039/c2cc31294h