Technology Process of C18H22N2O5
There total 7 articles about C18H22N2O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium osmate(VI) dihydrate; 4-methylmorpholine N-oxide;
In
N,N-dimethyl-formamide;
DOI:10.1002/chem.201200733
- Guidance literature:
-
Multi-step reaction with 4 steps
1: pancreatin from porcine pancreas; triethylamine / acetone / 23 h / 20 °C / Resolution of racemate; Enzymatic reaction
2: di-isopropyl azodicarboxylate; triphenylphosphine / acetonitrile / -40 - 20 °C / Inert atmosphere
3: methanol; sodium hydroxide / 20 °C
4: potassium osmate(VI) dihydrate; 4-methylmorpholine N-oxide / N,N-dimethyl-formamide
With
methanol; di-isopropyl azodicarboxylate; potassium osmate(VI) dihydrate; pancreatin from porcine pancreas; 4-methylmorpholine N-oxide; triethylamine; triphenylphosphine; sodium hydroxide;
In
N,N-dimethyl-formamide; acetone; acetonitrile;
2: Mitsunobu reaction;
DOI:10.1002/chem.201200733
- Guidance literature:
-
Multi-step reaction with 2 steps
1: methanol; sodium hydroxide / 20 °C
2: potassium osmate(VI) dihydrate; 4-methylmorpholine N-oxide / N,N-dimethyl-formamide
With
methanol; potassium osmate(VI) dihydrate; 4-methylmorpholine N-oxide; sodium hydroxide;
In
N,N-dimethyl-formamide;
DOI:10.1002/chem.201200733
