Technology Process of C60H60N2O4
There total 4 articles about C60H60N2O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
trifuran-2-yl-phosphane; palladium diacetate; silver carbonate;
In
o-xylene;
at 130 ℃;
for 18h;
Inert atmosphere;
DOI:10.1021/jo401061g
- Guidance literature:
-
Multi-step reaction with 3 steps
1: ethanol; toluene / 3 h / Inert atmosphere; Reflux
2: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere
3: palladium diacetate; trifuran-2-yl-phosphane; silver carbonate / o-xylene / 18 h / 130 °C / Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; trifuran-2-yl-phosphane; palladium diacetate; triethylamine; silver carbonate;
In
tetrahydrofuran; ethanol; o-xylene; toluene;
2: |Sonogashira Cross-Coupling;
DOI:10.1021/jo401061g
- Guidance literature:
-
Multi-step reaction with 3 steps
1: ethanol; toluene / 3 h / Inert atmosphere; Reflux
2: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere
3: palladium diacetate; trifuran-2-yl-phosphane; silver carbonate / o-xylene / 18 h / 130 °C / Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; trifuran-2-yl-phosphane; palladium diacetate; triethylamine; silver carbonate;
In
tetrahydrofuran; ethanol; o-xylene; toluene;
2: |Sonogashira Cross-Coupling;
DOI:10.1021/jo401061g
