N-phenylmethoxycarbonyl-1-aminoethyl sulfonic acid

Base Information

• Chemical Name: N-phenylmethoxycarbonyl-1-aminoethyl sulfonic acid
• CAS No.: 62554-01-2
• Molecular Formula: C₁₀H₁₃NO₅S
• Molecular Weight: 259.283
• Mol file: 62554-01-2.mol

Synonyms:

Chemical Property of N-phenylmethoxycarbonyl-1-aminoethyl sulfonic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-phenylmethoxycarbonyl-1-aminoethyl sulfonic acid

There total 1 articles about N-phenylmethoxycarbonyl-1-aminoethyl sulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-Aminoethanesulfonic acid (1636-31-3) + benzyl chloroformate (501-53-1,94274-21-2) → N-phenylmethoxycarbonyl-1-aminoethyl sulfonic acid (62554-01-2)

Guidance literature:

With sodium hydroxide; sodium hydrogencarbonate; sodium carbonate; at 20 ℃;

DOI:10.1016/j.bmcl.2005.08.055

Reference yield:

N-phenylmethoxycarbonyl-1-aminoethyl sulfonic acid (62554-01-2) → 2-(1-benzyloxycarbonylamino-ethanesulfonyloxy)-propionic acid methyl ester

Guidance literature:

Multi-step reaction with 2 steps

1: SOCl₂ / CHCl₃

2: 32 percent / Et₃N / CHCl₃ / 120 h / 20 °C

With thionyl chloride; triethylamine; In chloroform;

DOI:10.1016/j.bmcl.2005.08.055

Reference yield:

N-phenylmethoxycarbonyl-1-aminoethyl sulfonic acid (62554-01-2) → 2-(1-benzyloxycarbonylamino-ethanesulfonylamino)-propionic acid methyl ester

Guidance literature:

Multi-step reaction with 2 steps

1: SOCl₂ / CHCl₃

2: 28 percent / Et₃N / CHCl₃ / 192 h / 20 °C

With thionyl chloride; triethylamine; In chloroform;

DOI:10.1016/j.bmcl.2005.08.055

upstream raw materials:

1-Aminoethanesulfonic acid

benzyl chloroformate

Refernces