tricyclo<10.4.0.0^4,9>hexadeca-1(12),4(9)-diene-6,7:14,15-bis(N-phenyldicarboximide)

Base Information

• Chemical Name: tricyclo<10.4.0.0^4,9>hexadeca-1(12),4(9)-diene-6,7:14,15-bis(N-phenyldicarboximide)
• CAS No.: 72525-22-5
• Molecular Formula: C₃₂H₃₀N₂O₄
• Molecular Weight: 506.601

Synonyms:

Chemical Property of tricyclo<10.4.0.0^4,9>hexadeca-1(12),4(9)-diene-6,7:14,15-bis(N-phenyldicarboximide)

Chemical Property:

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Technology Process of tricyclo<10.4.0.0^4,9>hexadeca-1(12),4(9)-diene-6,7:14,15-bis(N-phenyldicarboximide)

There total 3 articles about tricyclo<10.4.0.0^4,9>hexadeca-1(12),4(9)-diene-6,7:14,15-bis(N-phenyldicarboximide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,4-dibromo-2,3-bis-bromomethyl-but-2-ene (30432-16-7) → tricyclo<10.4.0.04,9>hexadeca-1(12),4(9)-diene-6,7:14,15-bis(N-phenyldicarboximide) (72525-22-5)

Guidance literature:

Multi-step reaction with 3 steps

1: 73 percent / zinc-copper couple / diethyl ether; hexamethylphosphoric acid triamide / 4.5 h / Heating

2: zinc-copper couple / dimethylformamide / 2 h / Ambient temperature

3: benzene

With zinc copper; In N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; N,N-dimethyl-formamide; benzene;

DOI:10.1021/jo01293a021

Reference yield:

2,3-bis(bromomethyl)-1,3-butadiene (18214-55-6) → tricyclo<10.4.0.04,9>hexadeca-1(12),4(9)-diene-6,7:14,15-bis(N-phenyldicarboximide) (72525-22-5)

Guidance literature:

Multi-step reaction with 2 steps

1: zinc-copper couple / dimethylformamide / 2 h / Ambient temperature

2: benzene

With zinc copper; In N,N-dimethyl-formamide; benzene;

DOI:10.1021/jo01293a021

Reference yield:

N-phenyl-maleimide (941-69-5) + 1,2,5,6-tetra-exo-methylene-cyclooctane (27567-69-7) → tricyclo<10.4.0.04,9>hexadeca-1(12),4(9)-diene-6,7:14,15-bis(N-phenyldicarboximide) (72525-22-5)

Guidance literature:

In benzene;

DOI:10.1021/jo01293a021

upstream raw materials:

N-phenyl-maleimide

1,2,5,6-tetra-exo-methylene-cyclooctane

1,4-dibromo-2,3-bis-bromomethyl-but-2-ene

2,3-bis(bromomethyl)-1,3-butadiene

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