1-(1-methyl-1-phenylethyl)cyclobutene

Base Information

Chemical Name:1-(1-methyl-1-phenylethyl)cyclobutene
CAS No.:97452-40-9
Molecular Formula:C₁₃H₁₆
Molecular Weight:172.27
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(1-methyl-1-phenylethyl)cyclobutene

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Technology Process of 1-(1-methyl-1-phenylethyl)cyclobutene

There total 3 articles about 1-(1-methyl-1-phenylethyl)cyclobutene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 617-94-7
1-methyl-1-phenylethyl alcohol

: 97452-40-9
1-(1-methyl-1-phenylethyl)cyclobutene

Guidance literature:: Multi-step reaction with 3 steps

1: 96.5 percent / 70percent HClO₄ / benzene / 1 h / Heating

2: 1.) lithium naphthalene / 1.) THF, -65 deg C then up to -30 deg C, 1 h; 2.) THF, -60 deg C, 2 h; -30 deg C, 1 h, then RT

3: 31 percent Spectr_. / dimethylsulfoxide / 1.5 h / 160 - 170 °C

With perchloric acid; lithium dihydronaphthylide radical; In dimethyl sulfoxide; benzene;
DOI:10.1016/S0040-4020(01)96434-8

Reference yield:

: 4148-93-0
2-phenyl-2-propyl phenyl sulfide

: 97452-40-9
1-(1-methyl-1-phenylethyl)cyclobutene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) lithium naphthalene / 1.) THF, -65 deg C then up to -30 deg C, 1 h; 2.) THF, -60 deg C, 2 h; -30 deg C, 1 h, then RT

2: 31 percent Spectr_. / dimethylsulfoxide / 1.5 h / 160 - 170 °C

With lithium dihydronaphthylide radical; In dimethyl sulfoxide;
DOI:10.1016/S0040-4020(01)96434-8

Reference yield:

: 97452-37-4
1-(1-phenyl-1-methylethyl)cyclobutanol

: 19960-97-5
5,5-dimethyl-1-phenylcyclopentene

: 97452-40-9
1-(1-methyl-1-phenylethyl)cyclobutene

Guidance literature:: In dimethyl sulfoxide; at 160 - 170 ℃; for 1.5h; Title compound not separated from byproducts;
DOI:10.1016/S0040-4020(01)96434-8