bicyclo<2.2.0>hex-5-ene-2,3-dicarboxylic anhydride

Base Information

Chemical Name:bicyclo<2.2.0>hex-5-ene-2,3-dicarboxylic anhydride
CAS No.:68366-13-2
Molecular Formula:C₈H₆O₃
Molecular Weight:150.134
Hs Code.:

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Chemical Property of bicyclo<2.2.0>hex-5-ene-2,3-dicarboxylic anhydride

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Technology Process of bicyclo<2.2.0>hex-5-ene-2,3-dicarboxylic anhydride

There total 6 articles about bicyclo<2.2.0>hex-5-ene-2,3-dicarboxylic anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1515-19-1
cis-cyclohexa-3,5-diene-1,2-dicarboxylic anhydride

: 3097-60-7,68366-13-2
bicyclo<2.2.0>hex-5-ene-2,3-dicarboxylic anhydride

Guidance literature:: With mercury; In diethyl ether; at 20 ℃; for 27h; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.macromol.8b02754

Reference yield:

: 88-99-3,73607-73-5
benzene-1,2-dicarboxylic acid

: 3097-60-7,68366-13-2
bicyclo<2.2.0>hex-5-ene-2,3-dicarboxylic anhydride

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid; sodium acetate; sulfuric acid; sodium amalgam / water / Inert atmosphere; Schlenk technique

2: acetic anhydride / 1 h / 100 °C / Inert atmosphere; Schlenk technique

3: mercury / diethyl ether / 27 h / 20 °C / Inert atmosphere; Schlenk technique

With sulfuric acid; sodium amalgam; sodium acetate; acetic anhydride; acetic acid; mercury; In diethyl ether; water;
DOI:10.1021/acs.macromol.8b02754

Reference yield:

: 5675-13-8,22919-28-4,26554-23-4
trans-cyclohexa-3,5-diene-1,2-dicarboxylic acid

: 3097-60-7,68366-13-2
bicyclo<2.2.0>hex-5-ene-2,3-dicarboxylic anhydride

Guidance literature:: Multi-step reaction with 2 steps

1: acetic anhydride / 1 h / 100 °C / Inert atmosphere; Schlenk technique

2: mercury / diethyl ether / 27 h / 20 °C / Inert atmosphere; Schlenk technique

With acetic anhydride; mercury; In diethyl ether;
DOI:10.1021/acs.macromol.8b02754