Technology Process of C19H30O3
There total 2 articles about C19H30O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
boron trifluoride diethyl etherate;
In
dichloromethane;
at -78 ℃;
for 2h;
optical yield given as %de;
diastereoselective reaction;
Inert atmosphere;
DOI:10.1039/c2cc34187e
- Guidance literature:
-
Multi-step reaction with 3 steps
1: diisobutylaluminium hydride / dichloromethane / 2 h / -78 - -10 °C / Inert atmosphere
2: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1 h / 0 °C / Inert atmosphere
3: boron trifluoride diethyl etherate / dichloromethane / 2 h / -78 °C / Inert atmosphere
With
boron trifluoride diethyl etherate; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane;
In
dichloromethane;
DOI:10.1039/c2cc34187e
- Guidance literature:
-
With
2,6-dimethylpyridine;
In
dichloromethane;
at -78 ℃;
for 1h;
Inert atmosphere;
DOI:10.1039/c2cc34187e