Copper, [3-(ethoxycarbonyl)phenyl]-

Base Information

Chemical Name:Copper, [3-(ethoxycarbonyl)phenyl]-
CAS No.:139732-19-7
Molecular Formula:C₉H₉CuO₂
Molecular Weight:212.715
Hs Code.:

Synonyms:

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Chemical Property of Copper, [3-(ethoxycarbonyl)phenyl]-

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Technology Process of Copper, [3-(ethoxycarbonyl)phenyl]-

There total 2 articles about Copper, [3-(ethoxycarbonyl)phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 56667-47-1
Cu⁽¹⁺⁾*I^(1-)*P(C₂H₅)3=CuI*P(C₂H₅)3

: 58313-23-8
3-iodobenzoic acid methyl ester

: 139732-19-7
CuC₆H₄COOC₂H₅

Guidance literature:: With lithium naphthalide or lithium biphenylide; In 1,2-dimethoxyethane; byproducts: CuI; soln. of copper salt in DME quickly injected into stirring soln. of lithium salt (under Ar, via syringe, 5 min); addn. of alkyl halobenzoate to active Cu in DME (0°C, Cu/RX ratio = 3/1); stirring for 20 min;; not isolated; detn. by GC of secondary organic products;;
DOI:10.1021/om00040a028

Reference yield:

: 56667-47-1
Cu⁽¹⁺⁾*I^(1-)*P(C₂H₅)3=CuI*P(C₂H₅)3

: 24398-88-7
ethyl 3-bromobenzoate

: 139732-19-7
CuC₆H₄COOC₂H₅

Guidance literature:: With lithium naphthalide or lithium biphenylide; In tetrahydrofuran; byproducts: CuBr; soln. of copper salt in THF quickly injected into stirring soln. of lithium salt (under Ar, via syringe, 5 min); addn. of alkyl halobenzoate to active Cu in THF (0°C, Cu/RX ratio = 3/1); stirring for 20 min;; not isolated; detn. by GC of secondary organic products;;
DOI:10.1021/om00040a028