butyl<2-(diphenylphosphino)phenyl>phenylphosphine

Base Information

Chemical Name:butyl<2-(diphenylphosphino)phenyl>phenylphosphine
CAS No.:153041-63-5
Molecular Formula:C₂₈H₂₈P₂
Molecular Weight:426.478
Hs Code.:

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Chemical Property of butyl<2-(diphenylphosphino)phenyl>phenylphosphine

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Technology Process of butyl<2-(diphenylphosphino)phenyl>phenylphosphine

There total 1 articles about butyl<2-(diphenylphosphino)phenyl>phenylphosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10251-55-5
butyl(phenyl)phosphine

: 35035-62-2
diphenyl (2‐chlorophenyl) phosphine

: 153041-63-5
butyl<2-(diphenylphosphino)phenyl>phenylphosphine

Guidance literature:: With sodium; Yield given. Multistep reaction; 1.) THF, reflux, 1 h; reflux, 10 min, 2.) THF, -78 deg C to r.t., 2 h; reflux, 2 h;

Reference yield: 75.0%

: 81098-04-6
{NiC₄N₂S₂(Triphenylphosphin)2}

: 153041-63-5
butyl<2-(diphenylphosphino)phenyl>phenylphosphine

: 153148-03-9
{Ni(cis-1,2-dicyanoethene-1,2-dithiolato^(2-)-S,S')(C₆H₄(PBuPh)(PPh₂)-1,2)}

Guidance literature:: In acetone; under N2, stirred for 30 min; filtered, solvent reduced in volume, recrystd. (CH2Cl2/ethanol), twice recrystd. (CH2Cl2/diethyl ether), dried in vac.; elem. anal.;
DOI:10.1039/DT9930003593

Reference yield: 49.0%

: nickel(II) perchlorate hexahydrate

: 153041-63-5
butyl<2-(diphenylphosphino)phenyl>phenylphosphine

: bis{1-(n-butylphenylphosphino)-2-(diphenylphosphino)benzene-P,P'}nickel(II) diperchlorate

Guidance literature:: In dichloromethane; water; a soln. of the phosphine in CH2Cl2 was added to an aq. soln. of Ni(ClO4)2, stirred for 30 min; organic layer was separated, washed with water, dried over MgSO4, addn. of Et2O, recrystd. from CH2Cl2-Et2O, dried in vac.; elem. anal.;
DOI:10.1039/DT9940001231