4,4'-dibromo-2,2'-{[7-methyl-3,7,11,17-tetraazabicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-triene-3,11-diyl]dimethylene}diphenol

Base Information

• Chemical Name: 4,4'-dibromo-2,2'-{[7-methyl-3,7,11,17-tetraazabicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-triene-3,11-diyl]dimethylene}diphenol
• CAS No.: 817161-25-4
• Molecular Formula: C₂₈H₃₄Br₂N₄O₂
• Molecular Weight: 618.412
• Mol file: 817161-25-4.mol

Synonyms:

Chemical Property of 4,4'-dibromo-2,2'-{[7-methyl-3,7,11,17-tetraazabicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-triene-3,11-diyl]dimethylene}diphenol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4,4'-dibromo-2,2'-{[7-methyl-3,7,11,17-tetraazabicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-triene-3,11-diyl]dimethylene}diphenol

There total 2 articles about 4,4'-dibromo-2,2'-{[7-methyl-3,7,11,17-tetraazabicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-triene-3,11-diyl]dimethylene}diphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.7%

4-bromo-phenol (106-41-2) + 7-methyl-3,7,11,17-tetraaza-bicyclo[11.3.1]heptadeca-1(16),13(17),14-triene-3,11-dicarbaldehyde → 4,4'-dibromo-2,2'-{[7-methyl-3,7,11,17-tetraazabicyclo[11.3.1]heptadeca-1(17),13,15-triene-3,11-diyl]dimethylene}diphenol (817161-25-4)

Guidance literature:

In benzene; for 21h; Heating;

DOI:10.1002/hlca.200490235

Reference yield:

7-methyl-3,7,11,17-tetraazabicyclo-[11.3.1]heptadeca-1(17),13,15-triene (106202-21-5) → 4,4'-dibromo-2,2'-{[7-methyl-3,7,11,17-tetraazabicyclo[11.3.1]heptadeca-1(17),13,15-triene-3,11-diyl]dimethylene}diphenol (817161-25-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 100 percent / methanol / 20 °C

2: 74.7 percent / benzene / 21 h / Heating

In methanol; benzene;

DOI:10.1002/hlca.200490235

upstream raw materials:

4-bromo-phenol

7-methyl-3,7,11,17-tetraazabicyclo-[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-triene