[OsH₂(CS₂(CH₃))(NO)(P(C₆H₅)3)2]

Base Information

Chemical Name:[OsH₂(CS₂(CH₃))(NO)(P(C₆H₅)3)2]
CAS No.:105032-92-6
Molecular Formula:C₃₈H₃₅NOOsP₂S₂
Molecular Weight:837.982
Hs Code.:

[OsH<sub>2</sub>(CS<sub>2</sub>(CH<sub>3</sub>))(NO)(P(C<sub>6</sub>H<sub>5</sub>)3)2]

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [OsH₂(CS₂(CH₃))(NO)(P(C₆H₅)3)2]

Chemical Property:

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Technology Process of [OsH₂(CS₂(CH₃))(NO)(P(C₆H₅)3)2]

There total 1 articles about [OsH₂(CS₂(CH₃))(NO)(P(C₆H₅)3)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: [OsI(-eta.2-CS₂Me)(NO)(PPh₃)2]PF₆

: 105032-92-6
[OsH₂(CS₂(CH₃))(NO)(P(C₆H₅)3)2]

Guidance literature:: With sodium tetrahydroborate; In ethanol; (N2); a suspn. of PF6 in ethanol is treated with a filtered soln. of NaBH4 in ethanol at 0°C and stirred at room temp. for 15 min; addn. of H2O, stirring (5 min), filtration of ppt., washing (H2O, ethanol, 2*, hexane, 2*), drying (vac.), recrystn. (CH2Cl2/ethanol); elem. anal.;
DOI:10.1016/S0022-328X(00)99663-3

Reference yield:

: 105032-92-6
[OsH₂(CS₂(CH₃))(NO)(P(C₆H₅)3)2]

: 105032-94-8
OsCl(NO)(CS)(P(C₆H₅)3)2

Guidance literature:: With hydrogenchloride; In not given; (N2); silica gel;
DOI:10.1016/S0022-328X(00)99663-3

Reference yield:

: 105032-92-6
[OsH₂(CS₂(CH₃))(NO)(P(C₆H₅)3)2]

: 105032-98-2
OsI₂(NO)(CS)(P(C₆H₅)3)2⁽¹⁺⁾*I₃^(1-)=OsI₂(NO)(CS)(P(C₆H₅)3)2I₃

Guidance literature:: With iodine; In toluene; (N2); a suspn. of OsH2(CS2Me)(NO)(PPh3)2 in toluene at 0°C is treated dropwise with a cooled (0°C) soln. of I2 in toluene during ca. 5 min, the mixt. is stirred for 1 h and cooled to -30°C overnight, blood-red ppt.; filtration, washing (toluene, 0°C, hexane, 3*); elem. anal.;
DOI:10.1016/S0022-328X(00)99663-3