Mo2(O)(μ-O)(μ-C4Ph4)(η-C5H5)2

Base Information

• Chemical Name: Mo2(O)(μ-O)(μ-C4Ph4)(η-C5H5)2
• CAS No.: 212250-49-2
• Molecular Formula: C₃₈H₃₀Mo₂O₂
• Molecular Weight: 710.535

Synonyms:

Chemical Property of Mo2(O)(μ-O)(μ-C4Ph4)(η-C5H5)2

Chemical Property:

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Technology Process of Mo2(O)(μ-O)(μ-C4Ph4)(η-C5H5)2

There total 2 articles about Mo2(O)(μ-O)(μ-C4Ph4)(η-C5H5)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

cyclopentadienylmolybdenum tricarbonyl dimer + diphenyl acetylene (501-65-5) → Mo2(O)(μ-O)(μ-C4Ph4)(η-C5H5)2 (212250-49-2)

Guidance literature:

With air; In octane; refluxing Mo-complex with excess alkyne, solvent removal (vac.), dissoln. in CH2Cl2, stirring in air for 1 h; chromy. (SiO2, CH2Cl2/petroleum ether=1:1, then CH2Cl2/Me2CO=9:1);

DOI:10.1016/S0022-328X(96)06834-9

Reference yield:

Mo2(CO)(μ-C4Ph4)(η-C5H5)2 → Mo2(O)(μ-O)(μ-C4Ph4)(η-C5H5)2 (212250-49-2)

Guidance literature:

With air; In dichloromethane; exposure of CH2Cl2 soln. of educt to air; elem. anal.;

Reference yield: 29.0%

dicobalt octacarbonyl + Mo2(O)(μ-O)(μ-C4Ph4)(η-C5H5)2 (212250-49-2) → CoMo(CO)4(μ-C4Ph4)(η-C5H5)

Guidance literature:

In toluene; refluxing Mo-complex with excess of Co-complex for 1.25 h; chromy. (SiO2, CH2Cl2/petroleum ether=1:9, then 1:4); further unidentified product;

DOI:10.1016/S0022-328X(96)06834-9

upstream raw materials:

diphenyl acetylene

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