Cp*TiCl₂[N(2,6-Me₂C₆H₃)(SiMe₃)]

Base Information

• Chemical Name: Cp*TiCl₂[N(2,6-Me₂C₆H₃)(SiMe₃)]
• CAS No.: 443288-64-0
• Molecular Formula: C₂₁H₃₃Cl₂NSiTi
• Molecular Weight: 446.371

Synonyms:

Chemical Property of Cp*TiCl₂[N(2,6-Me₂C₆H₃)(SiMe₃)]

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Technology Process of Cp*TiCl₂[N(2,6-Me₂C₆H₃)(SiMe₃)]

There total 1 articles about Cp*TiCl₂[N(2,6-Me₂C₆H₃)(SiMe₃)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

lithium-N-(2,6-dimethylphenyl)-trimethylsilylamide + Cp*TiCl3 (12129-06-5) → Cp*TiCl2[N(2,6-Me2C6H3)(SiMe3)] (443288-64-0)

Guidance literature:

In toluene; under N2 atm. to Cp*TiCl3 in toluene at -30°C was added LiN(2,6-Me2C6H3)(SiMe3), warmed slowly to room temp. and heated at 110°C for 12 h; react. mixt. was filtered, soln. was evapd. in vacuo, residue was extd. with n-hexane at room temp., extract was concd. and cooled to -30°C; elem. anal.;

DOI:10.1021/om020179h

upstream raw materials:

Cp*TiCl₃

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