benzyl (6R,8S,11S,14S)-8-amino-14-[4-(benzyloxy)benzyl]-11-({4,4'-bis(benzyloxy)-3'-[2-{[(benzyloxy)carbonyl]amino}-3-oxo-3-(pentafluorphenoxy)propyl]biphenyl-3-yl}methyl)-6-hydroxy-3,9,12-trioxo-1-phenyl-2-oxa-4,10,13-triazapentadecan-15-oate hydrochloride

Base Information

• Chemical Name: benzyl (6R,8S,11S,14S)-8-amino-14-[4-(benzyloxy)benzyl]-11-({4,4'-bis(benzyloxy)-3'-[2-{[(benzyloxy)carbonyl]amino}-3-oxo-3-(pentafluorphenoxy)propyl]biphenyl-3-yl}methyl)-6-hydroxy-3,9,12-trioxo-1-phenyl-2-oxa-4,10,13-triazapentadecan-15-oate hydrochloride
• CAS No.: 868073-50-1
• Molecular Formula: C₈₂H₇₄F₅N₅O₁₄*ClH
• Molecular Weight: 1484.97

Synonyms:

Chemical Property of benzyl (6R,8S,11S,14S)-8-amino-14-[4-(benzyloxy)benzyl]-11-({4,4'-bis(benzyloxy)-3'-[2-{[(benzyloxy)carbonyl]amino}-3-oxo-3-(pentafluorphenoxy)propyl]biphenyl-3-yl}methyl)-6-hydroxy-3,9,12-trioxo-1-phenyl-2-oxa-4,10,13-triazapentadecan-15-oate hydrochloride

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Technology Process of benzyl (6R,8S,11S,14S)-8-amino-14-[4-(benzyloxy)benzyl]-11-({4,4'-bis(benzyloxy)-3'-[2-{[(benzyloxy)carbonyl]amino}-3-oxo-3-(pentafluorphenoxy)propyl]biphenyl-3-yl}methyl)-6-hydroxy-3,9,12-trioxo-1-phenyl-2-oxa-4,10,13-triazapentadecan-15-oate hydrochloride

There total 1 articles about benzyl (6R,8S,11S,14S)-8-amino-14-[4-(benzyloxy)benzyl]-11-({4,4'-bis(benzyloxy)-3'-[2-{[(benzyloxy)carbonyl]amino}-3-oxo-3-(pentafluorphenoxy)propyl]biphenyl-3-yl}methyl)-6-hydroxy-3,9,12-trioxo-1-phenyl-2-oxa-4,10,13-triazapentadecan-15-oate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzyl (6R,8S,11S,14S)-14-[4-(benzyloxy)benzyl]-11-({4,4'-bis(benzyloxy)-3'-[2-{[(benzyloxy)carbonyl]amino}-3-oxo-3-(pentafluorphenoxy)propyl]biphenyl-3-yl}methyl)-8-[(tert-butoxycarbonyl)amino]-6-hydroxy-3,9,12-trioxo-1-phenyl-2-oxa-4,10,13-triazapentadecan-15-oate (868073-49-8) → benzyl (6R,8S,11S,14S)-8-amino-14-[4-(benzyloxy)benzyl]-11-({4,4'-bis(benzyloxy)-3'-[2-{[(benzyloxy)carbonyl]amino}-3-oxo-3-(pentafluorphenoxy)propyl]biphenyl-3-yl}methyl)-6-hydroxy-3,9,12-trioxo-1-phenyl-2-oxa-4,10,13-triazapentadecan-15-oate hydrochloride (868073-50-1)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 3h;

Reference yield: 31.0%

benzyl (6R,8S,11S,14S)-8-amino-14-[4-(benzyloxy)benzyl]-11-({4,4'-bis(benzyloxy)-3'-[2-{[(benzyloxy)carbonyl]amino}-3-oxo-3-(pentafluorphenoxy)propyl]biphenyl-3-yl}methyl)-6-hydroxy-3,9,12-trioxo-1-phenyl-2-oxa-4,10,13-triazapentadecan-15-oate hydrochloride (868073-50-1) → benzyl O-benzyl-N-{[(8S,11S,14S)-5,17-bis(benzyloxy)-14-{[(benzyloxy)carbonyl]amino}-11-((2R)-3-{[(benzyloxy)carbonyl]amino}-2-hydroxypropyl)-10,13-dioxo-9,12-diazatricyclo[14.3 .1.1{2.6}]henicosa-1(20),2(21),3,5,16,18-hexaen-8-yl]carbonyl}-L-tyrosinate (868073-51-2)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 3h;

upstream raw materials:

benzyl (6R,8S,11S,14S)-14-[4-(benzyloxy)benzyl]-11-({4,4'-bis(benzyloxy)-3'-[2-{[(benzyloxy)carbonyl]amino}-3-oxo-3-(pentafluorphenoxy)propyl]biphenyl-3-yl}methyl)-8-[(tert-butoxycarbonyl)amino]-6-hydroxy-3,9,12-trioxo-1-phenyl-2-oxa-4,10,13-triazapentadecan-15-oate

Downstream raw materials:

benzyl O-benzyl-N-{[(8S,11S,14S)-5,17-bis(benzyloxy)-14-{[(benzyloxy)carbonyl]amino}-11-((2R)-3-{[(benzyloxy)carbonyl]amino}-2-hydroxypropyl)-10,13-dioxo-9,12-diazatricyclo[14.3 .1.1{2.6}]henicosa-1⁽²⁰⁾,2⁽²¹⁾,3,5,16,18-hexaen-8-yl]carbonyl}-L-tyrosinate

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