tricarbonyl[η3-N,4-dimethyl-2-phenyl-4,5-dihydropyrrole]iron(0)

Base Information

• Chemical Name: tricarbonyl[η3-N,4-dimethyl-2-phenyl-4,5-dihydropyrrole]iron(0)
• CAS No.: 606976-69-6
• Molecular Formula: C₁₅H₁₅FeNO₃
• Molecular Weight: 313.136
• Mol file: 606976-69-6.mol

Synonyms:

Chemical Property of tricarbonyl[η3-N,4-dimethyl-2-phenyl-4,5-dihydropyrrole]iron(0)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of tricarbonyl[η3-N,4-dimethyl-2-phenyl-4,5-dihydropyrrole]iron(0)

There total 1 articles about tricarbonyl[η3-N,4-dimethyl-2-phenyl-4,5-dihydropyrrole]iron(0) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

tetracarbonyl[(N-(2-methyl-2-propenyl)-N-methylamino)(phenyl)carbene]iron(0) + cis-tricarbonyl[(η2-N-(2-methyl-2-propenyl)-N-methylamino)(phenyl)carbene]iron(0) → tricarbonyl[η3-N,4-dimethyl-2-phenyl-4,5-dihydropyrrole]iron(0) (606149-59-1,606976-69-6)

Guidance literature:

In toluene; mixt. of Fe-complexes in toluene was heated to 100°C for 8 h under Ar; toluene was removed under reduced pressure, alumina column chromy. with CH2Cl2-light petroleum, solidified for several d in freezer; elem. anal.;

DOI:10.1021/om0301280