Technology Process of C25H30N2O4S
There total 4 articles about C25H30N2O4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
water; potassium carbonate;
In
methanol;
at 23 ℃;
for 14h;
Inert atmosphere;
DOI:10.1021/ja307851b
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium iodide / N,N-dimethyl-formamide / Reflux; Inert atmosphere
2: diethyl ether / 12 h / 0 - 4 °C / Inert atmosphere
3: (4R,4'R)-2,2'-(propane-2,2'diyl)bis(4-phenyl-4,5-dihydrooxazole); palladium (II) trifluoroacetate / methanol / -78 - 20 °C / Inert atmosphere
4: potassium carbonate; water / methanol / 14 h / 23 °C / Inert atmosphere
With
palladium (II) trifluoroacetate; water; potassium carbonate; (4R,4'R)-2,2'-(propane-2,2'diyl)bis(4-phenyl-4,5-dihydrooxazole); sodium iodide;
In
methanol; diethyl ether; N,N-dimethyl-formamide;
2: |Ene Reaction;
DOI:10.1021/ja307851b
- Guidance literature:
-
Multi-step reaction with 2 steps
1: (4R,4'R)-2,2'-(propane-2,2'diyl)bis(4-phenyl-4,5-dihydrooxazole); palladium (II) trifluoroacetate / methanol / -78 - 20 °C / Inert atmosphere
2: potassium carbonate; water / methanol / 14 h / 23 °C / Inert atmosphere
With
palladium (II) trifluoroacetate; water; potassium carbonate; (4R,4'R)-2,2'-(propane-2,2'diyl)bis(4-phenyl-4,5-dihydrooxazole);
In
methanol;
DOI:10.1021/ja307851b