[(C₅H₄)C(OH)(C₆H₅)2]2Ru

Base Information

Chemical Name:[(C₅H₄)C(OH)(C₆H₅)2]2Ru
CAS No.:162719-09-7
Molecular Formula:C₃₆H₃₀O₂Ru
Molecular Weight:595.703
Hs Code.:

[(C<sub>5</sub>H<sub>4</sub>)C(OH)(C<sub>6</sub>H<sub>5</sub>)2]2Ru

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Chemical Property of [(C₅H₄)C(OH)(C₆H₅)2]2Ru

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Technology Process of [(C₅H₄)C(OH)(C₆H₅)2]2Ru

There total 1 articles about [(C₅H₄)C(OH)(C₆H₅)2]2Ru which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1,1'-dibenzoylruthenocene

: 591-51-5
phenyllithium

: 162719-09-7
[(C₅H₄)C(OH)(C₆H₅)2]2Ru

Guidance literature:: With NH₄Cl; In diethyl ether; (Ar); soln. of PhLi added dropwise with stirring to soln. of (C5H4COPh)2Ru; after 1 h mixt. poured into satd. aq. soln. of NH4Cl; extd. (ether), dried (Na2SO4), evapd., crystd. (hexane/benzene); elem. anal.;
DOI:10.1007/BF00698254

Reference yield: 94.0%

: tetrafluoroboric acid

: 162719-09-7
[(C₅H₄)C(OH)(C₆H₅)2]2Ru

: 162761-45-7
[(C₆H₅)2(HO)CC₅H₄RuC₅H₄C(C₆H₅)2]⁽¹⁺⁾*BF₄^(1-) = [(C₆H₅)2(HO)CC₅H₄RuC₅H₄C(C₆H₅)2]BF₄

Guidance literature:: With ether; In dichloromethane; trifluoroacetic acid; soln. of HBF4/CF3COOH added to soln. of (C5H4C(OH)Ph2)2Ru in CH2Cl2; poured into abs. ether; filtered off, washed (ether);
DOI:10.1007/BF00698254

Reference yield: 90.0%

: 162719-09-7
[(C₅H₄)C(OH)(C₆H₅)2]2Ru

: 1493-13-6
trifluorormethanesulfonic acid

: 162719-08-6
[(C₆H₅)2(HO)CC₅H₄RuC₅H₄C(C₆H₅)2]⁽¹⁺⁾*[CF₃SO₃]^(1-) = [(C₆H₅)2(HO)CC₅H₄RuC₅H₄C(C₆H₅)2][CF₃SO₃]

Guidance literature:: With ether; In nitromethane; dichloromethane; CF3SO3H added to soln. of (C5H4C(OH)(C6H5)2)2Ru; mixt. poured into abs.ether, cooled overnight at -10 to -15°C;
DOI:10.1007/BF00698254