Nb(C₄H₂NC(C₆H₅)C₄H₂NC(C₆H₅)C₄H₂NC(C₆H₅)C₄H₂NC(C₆H₅))Br₂

Base Information

• Chemical Name: Nb(C₄H₂NC(C₆H₅)C₄H₂NC(C₆H₅)C₄H₂NC(C₆H₅)C₄H₂NC(C₆H₅))Br₂
• CAS No.: 89087-23-0
• Molecular Formula: C₄₄H₂₈Br₂N₄Nb
• Molecular Weight: 865.448
• Mol file: 89087-23-0.mol

Synonyms:

Chemical Property of Nb(C₄H₂NC(C₆H₅)C₄H₂NC(C₆H₅)C₄H₂NC(C₆H₅)C₄H₂NC(C₆H₅))Br₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Nb(C₄H₂NC(C₆H₅)C₄H₂NC(C₆H₅)C₄H₂NC(C₆H₅)C₄H₂NC(C₆H₅))Br₂

There total 1 articles about Nb(C₄H₂NC(C₆H₅)C₄H₂NC(C₆H₅)C₄H₂NC(C₆H₅)C₄H₂NC(C₆H₅))Br₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

Nb(C4H2NC(C6H5)C4H2NC(C6H5)C4H2NC(C6H5)C4H2NC(C6H5))Br3 (69133-82-0) → Nb(C4H2NC(C6H5)C4H2NC(C6H5)C4H2NC(C6H5)C4H2NC(C6H5))Br2 (89087-23-0)

Guidance literature:

With zinc amalgame; In tetrahydrofuran; under Ar, Nb-compd. treated with zinc amalgame over 30 min; evapd., washed with hexane, dried in vac.;

Reference yield:

Nb(C4H2NC(C6H5)C4H2NC(C6H5)C4H2NC(C6H5)C4H2NC(C6H5))Br2 (89087-23-0) → NbBr2(O2)(meso-tetraphenylporphinato)

Guidance literature:

With oxygen; In tetrahydrofuran; not isolated, detd. by ESR spectroscopy;

DOI:10.1039/c39830001454

upstream raw materials:

Nb(C₄H₂NC(C₆H₅)C₄H₂NC(C₆H₅)C₄H₂NC(C₆H₅)C₄H₂NC(C₆H₅))Br₃