N'-ethyl-2-(hydroxyimino)-N,N-dimethylacetimidamide hydrochloride

Base Information

• Chemical Name: N'-ethyl-2-(hydroxyimino)-N,N-dimethylacetimidamide hydrochloride
• CAS No.: 1293993-42-6
• Molecular Formula: C₆H₁₃N₃O*ClH
• Molecular Weight: 179.65
• Mol file: 1293993-42-6.mol

Synonyms:

Chemical Property of N'-ethyl-2-(hydroxyimino)-N,N-dimethylacetimidamide hydrochloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N'-ethyl-2-(hydroxyimino)-N,N-dimethylacetimidamide hydrochloride

There total 4 articles about N'-ethyl-2-(hydroxyimino)-N,N-dimethylacetimidamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

2-(benzyloxyimino)-N'-ethyl-N,N-dimethylacetimidamide hydrochloride (1293993-61-9) → N'-ethyl-2-(hydroxyimino)-N,N-dimethylacetimidamide hydrochloride (1293993-42-6)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; at 20 ℃;

DOI:10.1021/jm200054r

Reference yield:

CHF3O3S*C13H19N3O → N'-ethyl-2-(hydroxyimino)-N,N-dimethylacetimidamide hydrochloride (1293993-42-6)

Guidance literature:

Multi-step reaction with 2 steps

1: ion-exchange resin IRA-400 (Cl) / methanol; water

2: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 20 °C

With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; methanol; water;

DOI:10.1021/jm200054r

Reference yield:

C13H19N3O*HNO3 → N'-ethyl-2-(hydroxyimino)-N,N-dimethylacetimidamide hydrochloride (1293993-42-6)

Guidance literature:

Multi-step reaction with 2 steps

1: ion-exchange resin IRA-400 (Cl) / water

2: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 20 °C

With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; water;

DOI:10.1021/jm200054r

upstream raw materials:

2-(benzyloxyimino)-N'-ethyl-N,N-dimethylacetimidamide hydrochloride

Refernces

• 1、 Kalisiak, Jaros?aw,Ralph, Erik C.,Zhang, Jun,Cashman, John R.. "Amidine-Oximes: Reactivators for organophosphate exposure". . p. 3319 - 3330. Retrieved 2011/06/24.