C₁₇H₂₂O

Base Information

• Chemical Name: C₁₇H₂₂O
• CAS No.: 1432499-32-5
• Molecular Formula: C₁₇H₂₂O
• Molecular Weight: 242.361
• Mol file: 1432499-32-5.mol

Synonyms:

Chemical Property of C₁₇H₂₂O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₇H₂₂O

There total 3 articles about C₁₇H₂₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C13H16O (1432499-24-5) + 1-Bromo-2-butyne (3355-28-0) → C17H22O (1432499-32-5)

Guidance literature:

With indium; ammonium chloride; In methanol; water; at 20 ℃; for 12h; Inert atmosphere;

DOI:10.1021/ja4025963

Reference yield:

N,N-dimethyl-2-(2-methylphenyl)ethanamide (3917-57-5) → C17H22O (1432499-32-5)

Guidance literature:

Multi-step reaction with 3 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: 20 h / 20 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / toluene / 4 h / -78 - 0 °C / Inert atmosphere

3.1: ammonium chloride; indium / water; methanol / 12 h / 20 °C / Inert atmosphere

With indium; diisobutylaluminium hydride; ammonium chloride; lithium diisopropyl amide; In tetrahydrofuran; methanol; water; toluene;

DOI:10.1021/ja4025963

Reference yield:

C15H21NO (1432499-23-4) → C17H22O (1432499-32-5)

Guidance literature:

Multi-step reaction with 2 steps

1: diisobutylaluminium hydride / toluene / 4 h / -78 - 0 °C / Inert atmosphere

2: ammonium chloride; indium / water; methanol / 12 h / 20 °C / Inert atmosphere

With indium; diisobutylaluminium hydride; ammonium chloride; In methanol; water; toluene;

DOI:10.1021/ja4025963

upstream raw materials:

C₁₃H₁₆O

1-Bromo-2-butyne

N,N-dimethyl-2-(2-methylphenyl)ethanamide

C₁₅H₂₁NO