C₃₂H₄₂N₄O₈*ClH

Base Information

• Chemical Name: C₃₂H₄₂N₄O₈*ClH
• CAS No.: 1561903-67-0
• Molecular Formula: C₃₂H₄₂N₄O₈*ClH
• Molecular Weight: 647.168
• Mol file: 1561903-67-0.mol

Synonyms:

Chemical Property of C₃₂H₄₂N₄O₈*ClH

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₂H₄₂N₄O₈*ClH

There total 13 articles about C₃₂H₄₂N₄O₈*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

azacyclotridecane (295-03-4) → C32H42N4O8*ClH (1561903-67-0)

Guidance literature:

Multi-step reaction with 6 steps

1: triethylamine / N,N-dimethyl-formamide / 16 h / 70 °C / Inert atmosphere

2: lithium aluminium tetrahydride / diethyl ether / 0.25 h / 0 - 33 °C / Inert atmosphere

3: sodium iodide / dimethyl sulfoxide / 0.25 h / 20 °C / Inert atmosphere

4: methanol / 16 h / 20 °C

5: boron tribromide / dichloromethane / 1 h / -78 - 20 °C / Inert atmosphere

6: hydrogenchloride / methanol; diethyl ether; chloroform; pentane

With hydrogenchloride; lithium aluminium tetrahydride; boron tribromide; triethylamine; sodium iodide; In methanol; diethyl ether; dichloromethane; chloroform; dimethyl sulfoxide; N,N-dimethyl-formamide; pentane;

DOI:10.1039/c3ob42309c

Reference yield:

2-azacyclotridecanone (947-04-6,25038-74-8) → C32H42N4O8*ClH (1561903-67-0)

Guidance literature:

Multi-step reaction with 7 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere; Reflux

2: triethylamine / N,N-dimethyl-formamide / 16 h / 70 °C / Inert atmosphere

3: lithium aluminium tetrahydride / diethyl ether / 0.25 h / 0 - 33 °C / Inert atmosphere

4: sodium iodide / dimethyl sulfoxide / 0.25 h / 20 °C / Inert atmosphere

5: methanol / 16 h / 20 °C

6: boron tribromide / dichloromethane / 1 h / -78 - 20 °C / Inert atmosphere

7: hydrogenchloride / methanol; diethyl ether; chloroform; pentane

With hydrogenchloride; lithium aluminium tetrahydride; boron tribromide; triethylamine; sodium iodide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; chloroform; dimethyl sulfoxide; N,N-dimethyl-formamide; pentane;

DOI:10.1039/c3ob42309c

Reference yield:

3-(azacyclotridecan-1-yl)propan-1-amine (397263-15-9) → C32H42N4O8*ClH (1561903-67-0)

Guidance literature:

Multi-step reaction with 4 steps

1: sodium iodide / dimethyl sulfoxide / 0.25 h / 20 °C / Inert atmosphere

2: methanol / 16 h / 20 °C

3: boron tribromide / dichloromethane / 1 h / -78 - 20 °C / Inert atmosphere

4: hydrogenchloride / methanol; diethyl ether; chloroform; pentane

With hydrogenchloride; boron tribromide; sodium iodide; In methanol; diethyl ether; dichloromethane; chloroform; dimethyl sulfoxide; pentane;

DOI:10.1039/c3ob42309c

upstream raw materials:

azacyclotridecane

2-azacyclotridecanone

3-(azacyclotridecan-1-yl)propan-1-amine

4-allyl-2-methoxy-6-nitrophenol