(η-C5Me4)Fe(η-C5H4)CH2GePh2

Base Information

• Chemical Name: (η-C5Me4)Fe(η-C5H4)CH2GePh2
• CAS No.: 827611-57-4
• Molecular Formula: C₂₇H₂₈FeGe
• Molecular Weight: 480.956
• Mol file: 827611-57-4.mol

Synonyms:

Chemical Property of (η-C5Me4)Fe(η-C5H4)CH2GePh2

Chemical Property:

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Technology Process of (η-C5Me4)Fe(η-C5H4)CH2GePh2

There total 1 articles about (η-C5Me4)Fe(η-C5H4)CH2GePh2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

(η-C5(CH3)4CH2Li)Fe(η-C5H4Li)*2N,N,N',N'-tetramethylenediamine + dichlorodiphenylgermane (1613-66-7) → (η-C5Me4)Fe(η-C5H4)CH2GePh2 (827611-57-4)

Guidance literature:

In diethyl ether; under N2; soln. of GeCl2Ph2 in Et2O slowly added to suspn. of (η-C5Me4CH2Li)Fe(η-C5H4Li)*xTMEDA in Et2O at -78°C under stirring, mixt. allowed to warm to 25°C; soln. filtered, filtrate evapd. in vacuo for 24 h, residue recrystd. from hexanes at -30°C;

DOI:10.1021/om049650s

upstream raw materials:

dichlorodiphenylgermane