Carbon monoxide;toluene;tungsten

Base Information

Chemical Name:Carbon monoxide;toluene;tungsten
CAS No.:12128-82-4
Molecular Formula:C10H8 O3 W
Molecular Weight:360.022
Hs Code.:
DSSTox Substance ID:DTXSID40475258

Synonyms:DTXSID40475258

Suppliers and Price of Carbon monoxide;toluene;tungsten

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of Carbon monoxide;toluene;tungsten

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:0
Exact Mass:359.998277
Heavy Atom Count:14
Complexity:52

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=CC=C1.[C-]#[O+].[C-]#[O+].[C-]#[O+].[W]

Technology Process of Carbon monoxide;toluene;tungsten

There total 1 articles about Carbon monoxide;toluene;tungsten which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 81097-61-2
fac-W(CO)3(PMTA)

: 108-88-3,15644-74-3,16713-13-6
toluene

: 12128-82-4
(η(6)-toluene)tungsten(0) tricarbonyl

: 3030-47-5
N,N,N',N'',N'''-pentamethyldiethylenetriamine

Guidance literature:: In toluene; Schlenk techniques used; protective gas: N2; detailed description given; to stirred soln. of W(CO)3PMTA in toluene, BF3*OEt2 was added; reflux (2 h); cooling to room temp.;; filtration; evapn. to dryness; filtration of residue (through alumina/CH2Cl2 - hexane 1:4); evapn. to dryness; recrystn. (CH2Cl2/pentane/-20°C);;
DOI:10.1016/0022-328X(91)86100-5