Technology Process of C26H24N2O5S
There total 4 articles about C26H24N2O5S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: aluminum (III) chloride / 1,2-dichloro-ethane / 65 °C
2: potassium carbonate / N,N-dimethyl-formamide / 80 °C
3: sodium tetrahydroborate / methanol / 0.5 h
4: potassium carbonate / N,N-dimethyl-formamide / 1 h / 80 °C
5: trifluoroacetic acid / dichloromethane
With
aluminum (III) chloride; sodium tetrahydroborate; potassium carbonate; trifluoroacetic acid;
In
methanol; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2010.04.046
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / N,N-dimethyl-formamide / 80 °C
2: sodium tetrahydroborate / methanol / 0.5 h
3: potassium carbonate / N,N-dimethyl-formamide / 1 h / 80 °C
4: trifluoroacetic acid / dichloromethane
With
sodium tetrahydroborate; potassium carbonate; trifluoroacetic acid;
In
methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2010.04.046
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 80 °C
2: trifluoroacetic acid / dichloromethane
With
potassium carbonate; trifluoroacetic acid;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2010.04.046
