HU 913

Base Information

Chemical Name:HU 913
CAS No.:1309372-87-9
Molecular Formula:C₂₇H₄₀O₄
Molecular Weight:428.612
Hs Code.:

Synonyms:

Suppliers and Price of HU 913

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of HU 913

Chemical Property:

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Technology Process of HU 913

There total 6 articles about HU 913 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21286-54-4,39262-22-1
D-camphor-10-sulfonyl chloride

: 1309372-87-9
HU 913

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium carbonate; potassium permanganate / water / Reflux

2.1: potassium carbonate / N,N-dimethyl-formamide / 18 h / 20 °C / Inert atmosphere

3.1: lithium diisopropyl amide / tetrahydrofuran / -78 - 0 °C / Inert atmosphere

3.2: 18 h / 0 - 20 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 15 h / Inert atmosphere; Reflux

5.1: water; lithium hydroxide / methanol / 48 h / 200 °C

With potassium permanganate; tetrabutyl ammonium fluoride; water; sodium carbonate; potassium carbonate; lithium hydroxide; lithium diisopropyl amide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; 4.1: Suzuki Coupling;

Reference yield:

: 60526-81-0
1-(1',1'-dimethylheptyl)-3,5-dimethoxybenzene

: 1309372-87-9
HU 913

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 15 h / Inert atmosphere; Reflux

3.1: water; lithium hydroxide / methanol / 48 h / 200 °C

With n-butyllithium; tetrabutyl ammonium fluoride; water; lithium hydroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; hexane; 2.1: Suzuki Coupling;

Reference yield:

: 210641-38-6
(1R,4S)-7,7-dimethyl-2-oxo-bicyclo[2.2.1]heptane-1-carboxylic acid methyl ester

: 1309372-87-9
HU 913

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / -78 - 0 °C / Inert atmosphere

1.2: 18 h / 0 - 20 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 15 h / Inert atmosphere; Reflux

3.1: water; lithium hydroxide / methanol / 48 h / 200 °C

With tetrabutyl ammonium fluoride; water; lithium hydroxide; lithium diisopropyl amide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; 2.1: Suzuki Coupling;