C₂₃H₃₀N₂O₄

Base Information

Chemical Name:C₂₃H₃₀N₂O₄
CAS No.:1419075-26-5
Molecular Formula:C₂₃H₃₀N₂O₄
Molecular Weight:398.502
Hs Code.:

C<sub>23</sub>H<sub>30</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₃H₃₀N₂O₄

Chemical Property:

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Technology Process of C₂₃H₃₀N₂O₄

There total 12 articles about C₂₃H₃₀N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1419075-25-4
C₂₆H₃₈N₂O₆

: 1419075-26-5
C₂₃H₃₀N₂O₄

Guidance literature:: With methanesulfonic acid; In dichloromethane; for 1.5h; stereoselective reaction;
DOI:10.1002/ejoc.201200919

Reference yield:

: (R)-benzyl [1-(2-(2-(1,3-dioxoisoindolin-2-yl)ethyl)-1,3-dioxan-2-yl)propan-2-yl]carbamate

: 1419075-26-5
C₂₃H₃₀N₂O₄

Guidance literature:: Multi-step reaction with 10 steps

1.1: hydrazine hydrate / methanol / 2 h / Reflux

2.1: dmap; triethylamine / dichloromethane / 0 - 20 °C

2.2: 0.5 h / 0 - 20 °C

3.1: palladium 10% on activated carbon; ammonium formate / methanol / 3 h / Reflux

4.1: magnesium sulfate / dichloromethane / Reflux

4.2: 14 h / 40 °C

5.1: palladium 10% on activated carbon; ammonium formate / methanol / 2 h / Reflux

6.1: sodium carbonate / dichloromethane; water / 3 h / 20 °C

7.1: Amberlite IRA 401 / methanol

8.1: toluene / 3 h / Reflux

8.2: 1 h

9.1: lithium triethylborohydride / dichloromethane / 1 h / -78 °C

10.1: methanesulfonic acid / dichloromethane / 1.5 h

With dmap; methanesulfonic acid; palladium 10% on activated carbon; ammonium formate; lithium triethylborohydride; sodium carbonate; magnesium sulfate; hydrazine hydrate; triethylamine; In methanol; dichloromethane; water; toluene; 4.1: |Mannich Aminomethylation;
DOI:10.1002/ejoc.201200919

Reference yield:

: 1350922-84-7
(R)-benzyl [1-(2-(2-aminoethyl)-1,3-dioxan-2-yl)propan-2-yl]carbamate

: 1419075-26-5
C₂₃H₃₀N₂O₄

Guidance literature:: Multi-step reaction with 9 steps

1.1: dmap; triethylamine / dichloromethane / 0 - 20 °C

1.2: 0.5 h / 0 - 20 °C

2.1: palladium 10% on activated carbon; ammonium formate / methanol / 3 h / Reflux

3.1: magnesium sulfate / dichloromethane / Reflux

3.2: 14 h / 40 °C

4.1: palladium 10% on activated carbon; ammonium formate / methanol / 2 h / Reflux

5.1: sodium carbonate / dichloromethane; water / 3 h / 20 °C

6.1: Amberlite IRA 401 / methanol

7.1: toluene / 3 h / Reflux

7.2: 1 h

8.1: lithium triethylborohydride / dichloromethane / 1 h / -78 °C

9.1: methanesulfonic acid / dichloromethane / 1.5 h

With dmap; methanesulfonic acid; palladium 10% on activated carbon; ammonium formate; lithium triethylborohydride; sodium carbonate; magnesium sulfate; triethylamine; In methanol; dichloromethane; water; toluene; 3.1: |Mannich Aminomethylation;
DOI:10.1002/ejoc.201200919