C₅₀H₈₃N₇O₇Si₂

Base Information

Chemical Name:C₅₀H₈₃N₇O₇Si₂
CAS No.:1431217-31-0
Molecular Formula:C₅₀H₈₃N₇O₇Si₂
Molecular Weight:950.423
Hs Code.:

C<sub>50</sub>H<sub>83</sub>N<sub>7</sub>O<sub>7</sub>Si<sub>2</sub>

Synonyms:

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Chemical Property of C₅₀H₈₃N₇O₇Si₂

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Technology Process of C₅₀H₈₃N₇O₇Si₂

There total 8 articles about C₅₀H₈₃N₇O₇Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1454334-73-6
C₇H₁₅N₅O

: 1431217-31-0
C₅₀H₈₃N₇O₇Si₂

: 1431217-41-2
C₅₀H₈₃N₇O₇Si₂

Guidance literature:: Multi-step reaction with 3 steps

1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h

2: trifluoroacetic acid / dichloromethane / 1 h

3: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h

With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1039/c3cc40628h

Reference yield:

: 1431217-28-5
C₁₈H₃₄N₆O₄

: 1431217-31-0
C₅₀H₈₃N₇O₇Si₂

: 1431217-41-2
C₅₀H₈₃N₇O₇Si₂

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 1 h

2: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h

With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1039/c3cc40628h

Reference yield:

: 22818-40-2
D-4-hydroxyphenylglycine

: 1431217-31-0
C₅₀H₈₃N₇O₇Si₂

: 1431217-41-2
C₅₀H₈₃N₇O₇Si₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: acetic acid; Iodine monochloride / 72 h / 20 °C / Inert atmosphere

2.1: triethylamine / water; 1,4-dioxane

2.2: pH 2 - 3

3.1: sodium hydroxide / dichloromethane; water / 3 h / 0 - 20 °C

3.2: pH 2 - 3

4.1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 h / 20 °C / Inert atmosphere

5.1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; Iodine monochloride; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; 4.1: |Sonogashira Cross-Coupling;
DOI:10.1039/c3cc40628h