C₂₆H₃₃NO₅

Base Information

Chemical Name:C₂₆H₃₃NO₅
CAS No.:1579997-01-5
Molecular Formula:C₂₆H₃₃NO₅
Molecular Weight:439.552
Hs Code.:

C<sub>26</sub>H<sub>33</sub>NO<sub>5</sub>

Synonyms:

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Chemical Property of C₂₆H₃₃NO₅

Chemical Property:

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Technology Process of C₂₆H₃₃NO₅

There total 11 articles about C₂₆H₃₃NO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1579996-75-0
tert-butyl (2S,3S,4R)-3,4-bis(benzyloxy)-2-((R)-1-hydroxyallyl)-pyrrolidine-1-carboxylate

: 1579997-01-5
C₂₆H₃₃NO₅

Guidance literature:: With benzyl bromide; sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1039/c3ra47555g

Reference yield:

: (4R,5S,6R)-4,5-bis(benzyloxy)-6-(trityloxymethyl)tetrahydro-2H-pyran-2,3-diol

: 1579997-01-5
C₂₆H₃₃NO₅

Guidance literature:: Multi-step reaction with 10 steps

1: sodium periodate; sodium hydrogencarbonate / water; ethanol / 4 h / 20 °C / Inert atmosphere

2: sodium tetrahydroborate / methanol / 1.08 h / 0 - 20 °C / Inert atmosphere

3: triethylamine; dmap / dichloromethane / 0 °C / Inert atmosphere

4: neat (no solvent) / 2 h / 70 °C / Inert atmosphere

5: trifluoroacetic acid / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

6: hydrogen; 10 wt% Pd(OH)2 on carbon / methanol / 1 h / 20 °C / 760.05 Torr / Inert atmosphere

7: sodium carbonate / ethyl acetate / 2 h / 20 °C / Inert atmosphere

8: chromium(VI) oxide; acetic anhydride; pyridine / dichloromethane / 1.25 h / 0 - 20 °C / Inert atmosphere

9: potassium tert-butylate / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

10: benzyl bromide; sodium hydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

With pyridine; chromium(VI) oxide; dmap; sodium tetrahydroborate; sodium periodate; 10 wt% Pd(OH)2 on carbon; potassium tert-butylate; hydrogen; acetic anhydride; benzyl bromide; sodium hydride; sodium hydrogencarbonate; sodium carbonate; triethylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; ethyl acetate;
DOI:10.1039/c3ra47555g

Reference yield:

: 1579996-58-9
(2R,3S,4S)-3,4-bis(benzyloxy)-5-oxo-1-(trityloxy)pentan-2-yl formate

: 1579997-01-5
C₂₆H₃₃NO₅

Guidance literature:: Multi-step reaction with 9 steps

1: sodium tetrahydroborate / methanol / 1.08 h / 0 - 20 °C / Inert atmosphere

2: triethylamine; dmap / dichloromethane / 0 °C / Inert atmosphere

3: neat (no solvent) / 2 h / 70 °C / Inert atmosphere

4: trifluoroacetic acid / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

5: hydrogen; 10 wt% Pd(OH)2 on carbon / methanol / 1 h / 20 °C / 760.05 Torr / Inert atmosphere

6: sodium carbonate / ethyl acetate / 2 h / 20 °C / Inert atmosphere

7: chromium(VI) oxide; acetic anhydride; pyridine / dichloromethane / 1.25 h / 0 - 20 °C / Inert atmosphere

8: potassium tert-butylate / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

9: benzyl bromide; sodium hydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

With pyridine; chromium(VI) oxide; dmap; sodium tetrahydroborate; 10 wt% Pd(OH)2 on carbon; potassium tert-butylate; hydrogen; acetic anhydride; benzyl bromide; sodium hydride; sodium carbonate; triethylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate;
DOI:10.1039/c3ra47555g