Technology Process of 4,4'-(5,6-dimethyl-1H-benzo[d]imidazole-4,7-diyl)dibenzoic acid
There total 4 articles about 4,4'-(5,6-dimethyl-1H-benzo[d]imidazole-4,7-diyl)dibenzoic acid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
water; sodium hydroxide;
In
tetrahydrofuran; ethanol;
DOI:10.1039/c4cc00334a
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydroxide; potassium permanganate / tert-butyl alcohol; water
2: sulfuric acid
3: tetrakis(triphenylphosphine) palladium(0); potassium phosphate / 1,4-dioxane / 72 h / 100 °C / Inert atmosphere; Schlenk technique
4: water; sodium hydroxide / tetrahydrofuran; ethanol
With
potassium phosphate; potassium permanganate; tetrakis(triphenylphosphine) palladium(0); sulfuric acid; water; sodium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; ethanol; water; tert-butyl alcohol;
3: |Suzuki Coupling;
DOI:10.1039/c4cc00334a
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sulfuric acid
2: tetrakis(triphenylphosphine) palladium(0); potassium phosphate / 1,4-dioxane / 72 h / 100 °C / Inert atmosphere; Schlenk technique
3: water; sodium hydroxide / tetrahydrofuran; ethanol
With
potassium phosphate; tetrakis(triphenylphosphine) palladium(0); sulfuric acid; water; sodium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; ethanol;
2: |Suzuki Coupling;
DOI:10.1039/c4cc00334a
