3-bromo-2-chloro-7-iodoquinoline

Base Information

Chemical Name:3-bromo-2-chloro-7-iodoquinoline
CAS No.:2086768-49-0
Molecular Formula:C₉H₄BrClIN
Molecular Weight:368.399
Hs Code.:

Synonyms:

Suppliers and Price of 3-bromo-2-chloro-7-iodoquinoline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 2 raw suppliers

Chemical Property of 3-bromo-2-chloro-7-iodoquinoline

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-bromo-2-chloro-7-iodoquinoline

There total 6 articles about 3-bromo-2-chloro-7-iodoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.5%

: C₉H₅BrINO

: 2086768-49-0
3-bromo-2-chloro-7-iodoquinoline

Guidance literature:: With trichlorophosphate; In chloroform; at 80 ℃; for 12h;

Reference yield:

: 1354223-46-3
3-bromo-7-iodoquinoline

: 2086768-49-0
3-bromo-2-chloro-7-iodoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 96 h / 20 °C

2: trichlorophosphate / chloroform / 12 h / 80 °C

With 3-chloro-benzenecarboperoxoic acid; trichlorophosphate; In dichloromethane; chloroform;

Reference yield:

: 30450-62-5
7-nitro-1,2,3,4-tetrahydro-quinoline

: 2086768-49-0
3-bromo-2-chloro-7-iodoquinoline

Guidance literature:: Multi-step reaction with 6 steps

1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 3 h / 0 - 20 °C

2: N-Bromosuccinimide / acetic acid / 2 h / 110 °C

3: iron; ammonium chloride / ethanol; water / 2 h / 80 °C / Inert atmosphere

4: sodium nitrite; sodium iodide; sulfuric acid / water / 3 h / 0 - 60 °C

5: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C

6: trichlorophosphate / chloroform / 2 h / 80 °C

With N-Bromosuccinimide; sulfuric acid; iron; ammonium chloride; 3-chloro-benzenecarboperoxoic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium iodide; sodium nitrite; trichlorophosphate; In ethanol; dichloromethane; chloroform; water; acetic acid;