cis,cis-Dicyclohexyl-buta-1,3-dien

Base Information

• Chemical Name: cis,cis-Dicyclohexyl-buta-1,3-dien
• CAS No.: 16636-32-1
• Molecular Formula: C₁₆H₂₆
• Molecular Weight: 218.382
• Mol file: 16636-32-1.mol

Synonyms:

Chemical Property of cis,cis-Dicyclohexyl-buta-1,3-dien

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of cis,cis-Dicyclohexyl-buta-1,3-dien

There total 5 articles about cis,cis-Dicyclohexyl-buta-1,3-dien which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

vinylcyclohexane (695-12-5,25498-06-0) → cis,cis-Dicyclohexyl-buta-1,3-dien (16636-32-1)

Guidance literature:

Multi-step reaction with 4 steps

1: Br₂ / CCl₄

2: NaNH₂

3: CuCl, Me₂NCH₂CH₂NMe₂, O₂

4: (i) iBu₃B, (ii) AcOH

With N,N,N,N,-tetramethylethylenediamine; bromine; oxygen; sodium amide; copper(l) chloride; In tetrachloromethane;

DOI:10.1039/jr9650006669

Reference yield:

2-cyclohexylacetylene (931-48-6) → cis,cis-Dicyclohexyl-buta-1,3-dien (16636-32-1)

Guidance literature:

Multi-step reaction with 2 steps

1: CuCl, Me₂NCH₂CH₂NMe₂, O₂

2: (i) iBu₃B, (ii) AcOH

With N,N,N,N,-tetramethylethylenediamine; oxygen; copper(l) chloride;

DOI:10.1039/jr9650006669

Reference yield:

1,2-dibromo-1-cyclohexylethane (81602-60-0) → cis,cis-Dicyclohexyl-buta-1,3-dien (16636-32-1)

Guidance literature:

Multi-step reaction with 3 steps

1: NaNH₂

2: CuCl, Me₂NCH₂CH₂NMe₂, O₂

3: (i) iBu₃B, (ii) AcOH

With N,N,N,N,-tetramethylethylenediamine; oxygen; sodium amide; copper(l) chloride;

DOI:10.1039/jr9650006669

upstream raw materials:

1,4-dicyclohexylbuta-1,3-diyne

vinylcyclohexane

2-cyclohexylacetylene

1,2-dibromo-1-cyclohexylethane