Benzyl-O--(2->6)-O-(2-amino-3-O-<α,α-D2>benzyl-2-desoxy-β-D-glucopyranosyl)-(1->6)-2-amino-3,4-di-O-<α,α-D2>benzyl-2-desoxy-β-D-glucopyranosid-dihydrochlorid

Base Information

Chemical Name:Benzyl-O--(2->6)-O-(2-amino-3-O-<α,α-D2>benzyl-2-desoxy-β-D-glucopyranosyl)-(1->6)-2-amino-3,4-di-O-<α,α-D2>benzyl-2-desoxy-β-D-glucopyranosid-dihydrochlorid
CAS No.:106115-86-0
Molecular Formula:C₅₇H₇₀N₂O₂₀*2ClH
Molecular Weight:1182.06
Hs Code.:

Benzyl-O-<methyl-(4,5,7,8-tetra-O-acetyl-3-desoxy-α-D-manno-2-octulopyranosyl)onat>-(2->6)-O-(2-amino-3-O-<α,α-D2>benzyl-2-desoxy-β-D-glucopyranosyl)-(1->6)-2-amino-3,4-di-O-<α,α-D2>benzyl-2-desoxy-β-D-glucopyranosid-dihydrochlorid

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Chemical Property of Benzyl-O--(2->6)-O-(2-amino-3-O-<α,α-D2>benzyl-2-desoxy-β-D-glucopyranosyl)-(1->6)-2-amino-3,4-di-O-<α,α-D2>benzyl-2-desoxy-β-D-glucopyranosid-dihydrochlorid

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Technology Process of Benzyl-O--(2->6)-O-(2-amino-3-O-<α,α-D2>benzyl-2-desoxy-β-D-glucopyranosyl)-(1->6)-2-amino-3,4-di-O-<α,α-D2>benzyl-2-desoxy-β-D-glucopyranosid-dihydrochlorid

There total 10 articles about Benzyl-O--(2->6)-O-(2-amino-3-O-<α,α-D2>benzyl-2-desoxy-β-D-glucopyranosyl)-(1->6)-2-amino-3,4-di-O-<α,α-D2>benzyl-2-desoxy-β-D-glucopyranosid-dihydrochlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85382-87-2
methyl (4,5,7,8-tetra-O-acetyl-3-deoxy-α-D-manno-oct-2-ulopyranosyl bromide)onate

: 106115-86-0
Benzyl-O--(2->6)-O-(2-amino-3-O-<α,α-D2>benzyl-2-desoxy-β-D-glucopyranosyl)-(1->6)-2-amino-3,4-di-O-<α,α-D2>benzyl-2-desoxy-β-D-glucopyranosid-dihydrochlorid

Guidance literature:: Multi-step reaction with 2 steps

1: 30 percent / Ag₂CO₃, AgClO₄, drierite / CH₂Cl₂ / 18 h / 0 °C

2: 1.) H₂S, 2.) 0.5 N HCl / 1.) pyridine, H₂O, 8 h, 60 deg C, 2.) MeOH, 0 deg C

With hydrogenchloride; calcium sulfate; hydrogen sulfide; silver perchlorate; silver carbonate; In dichloromethane;

Reference yield:

: 106115-79-1
4,6-Di-O-acetyl-2-azido-3-O-<α,α-D2>benzyl-2-desoxy-α-D-glucopyranosylbromid

: 106115-86-0
Benzyl-O--(2->6)-O-(2-amino-3-O-<α,α-D2>benzyl-2-desoxy-β-D-glucopyranosyl)-(1->6)-2-amino-3,4-di-O-<α,α-D2>benzyl-2-desoxy-β-D-glucopyranosid-dihydrochlorid

Guidance literature:: Multi-step reaction with 4 steps

1: silver silicate, molecular sieve 4 Angstroem / CH₂Cl₂ / 2.5 h / -20 °C

2: 3.5 g / 2 N NaOMe / methanol; CH₂Cl₂ / 5 h / 40 °C

3: 30 percent / Ag₂CO₃, AgClO₄, drierite / CH₂Cl₂ / 18 h / 0 °C

4: 1.) H₂S, 2.) 0.5 N HCl / 1.) pyridine, H₂O, 8 h, 60 deg C, 2.) MeOH, 0 deg C

With hydrogenchloride; calcium sulfate; silver silicate; 4 A molecular sieve; hydrogen sulfide; sodium methylate; silver perchlorate; silver carbonate; In methanol; dichloromethane;

Reference yield:

: 106139-07-5
6-O-Acetyl-2-azido-3,4-di-O-<α,α-D2>benzyl-2-desoxy-α-D-glucopyranosylbromid

: 106115-86-0
Benzyl-O--(2->6)-O-(2-amino-3-O-<α,α-D2>benzyl-2-desoxy-β-D-glucopyranosyl)-(1->6)-2-amino-3,4-di-O-<α,α-D2>benzyl-2-desoxy-β-D-glucopyranosid-dihydrochlorid

Guidance literature:: Multi-step reaction with 6 steps

1: 82 percent / silver silicate, molecular sieve 4 Angstroem / CH₂Cl₂ / 2 h / -20 °C

2: 1 M NaOMe / CH₂Cl₂; methanol / 2 h

3: silver silicate, molecular sieve 4 Angstroem / CH₂Cl₂ / 2.5 h / -20 °C

4: 3.5 g / 2 N NaOMe / methanol; CH₂Cl₂ / 5 h / 40 °C

5: 30 percent / Ag₂CO₃, AgClO₄, drierite / CH₂Cl₂ / 18 h / 0 °C

6: 1.) H₂S, 2.) 0.5 N HCl / 1.) pyridine, H₂O, 8 h, 60 deg C, 2.) MeOH, 0 deg C

With hydrogenchloride; calcium sulfate; silver silicate; 4 A molecular sieve; hydrogen sulfide; sodium methylate; silver perchlorate; silver carbonate; In methanol; dichloromethane;