tri-p-tolylplumbyl-tri-p-tolylstannane

Base Information

Chemical Name:tri-p-tolylplumbyl-tri-p-tolylstannane
CAS No.:137715-72-1
Molecular Formula:C₄₂H₄₂PbSn
Molecular Weight:872.705
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tri-p-tolylplumbyl-tri-p-tolylstannane

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Technology Process of tri-p-tolylplumbyl-tri-p-tolylstannane

There total 1 articles about tri-p-tolylplumbyl-tri-p-tolylstannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 104026-64-4
(p-Tol)3PbLi

: 41269-16-3
tris(4-methylphenyl)tin(IV) iodide

: 137715-72-1
tri-p-tolylplumbyl-tri-p-tolylstannane

Guidance literature:: In tetrahydrofuran; diethyl ether; byproducts: LiI; dissolving of tri-o-tolyl tin iodide in abs. diethyl ether and cooling down with methanol/dry-ice at -78°C, then addn. of tri-p-tolylplumbyllithium soln. in THF within 1h; during 8 h stirring warming to -10°C;; removal of ppt., recrystn. from chloroform; elem. anal.;;
DOI:10.1016/0022-328X(91)80135-7