Technology Process of C23H19FN6O3
There total 11 articles about C23H19FN6O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate;
In
acetonitrile;
at 80 ℃;
DOI:10.1016/j.bmcl.2011.07.034
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium azide / N,N-dimethyl-formamide / 70 °C
2: triphenylphosphine / tetrahydrofuran; water / 50 °C
3: triethylamine / dichloromethane / 0 - 20 °C
4: iodine; silver trifluoroacetate / chloroform; acetonitrile
5: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate / acetonitrile / 80 °C
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium azide; iodine; silver trifluoroacetate; potassium carbonate; triethylamine; triphenylphosphine;
In
tetrahydrofuran; dichloromethane; chloroform; water; N,N-dimethyl-formamide; acetonitrile;
5: Suzuki coupling reaction;
DOI:10.1016/j.bmcl.2011.07.034
- Guidance literature:
-
Multi-step reaction with 3 steps
1: [bis(acetoxy)iodo]benzene / dichloromethane / 20 °C
2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,4-dioxane / 80 °C
3: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate / acetonitrile / 80 °C
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; [bis(acetoxy)iodo]benzene; potassium acetate; potassium carbonate;
In
1,4-dioxane; dichloromethane; acetonitrile;
2: Miyaura borylation / 3: Suzuki coupling reaction;
DOI:10.1016/j.bmcl.2011.07.034
