2-[(E)-2-[4-(1,4-dioxa-7,13-dithia-10-azacyclopentadec-10-yl)phenyl]vinyl]-3-(4-sulfonatobutyl)-1,3-benzothiazolium

Base Information

• Chemical Name: 2-[(E)-2-[4-(1,4-dioxa-7,13-dithia-10-azacyclopentadec-10-yl)phenyl]vinyl]-3-(4-sulfonatobutyl)-1,3-benzothiazolium
• CAS No.: 1068434-78-5
• Molecular Formula: C₂₉H₃₈N₂O₅S₄
• Molecular Weight: 622.895
• Mol file: 1068434-78-5.mol

Synonyms:

Chemical Property of 2-[(E)-2-[4-(1,4-dioxa-7,13-dithia-10-azacyclopentadec-10-yl)phenyl]vinyl]-3-(4-sulfonatobutyl)-1,3-benzothiazolium

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-[(E)-2-[4-(1,4-dioxa-7,13-dithia-10-azacyclopentadec-10-yl)phenyl]vinyl]-3-(4-sulfonatobutyl)-1,3-benzothiazolium

There total 1 articles about 2-[(E)-2-[4-(1,4-dioxa-7,13-dithia-10-azacyclopentadec-10-yl)phenyl]vinyl]-3-(4-sulfonatobutyl)-1,3-benzothiazolium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

4-(1,4-dioxa-7,13-dithia-10-azacyclopentadecan-10-yl) benzaldehyde (240797-82-4) + N-(δ-sulfonatobutyl)-2-methyl-benzothiazole (55526-95-9) → 2-[(E)-2-[4-(1,4-dioxa-7,13-dithia-10-azacyclopentadec-10-yl)phenyl]vinyl]-3-(4-sulfonatobutyl)-1,3-benzothiazolium (1068434-78-5)

Guidance literature:

With pyridine; In ethanol; for 30h; Heating;

DOI:10.1007/s11172-007-0082-4

Reference yield:

2-[(E)-2-[4-(1,4-dioxa-7,13-dithia-10-azacyclopentadec-10-yl)phenyl]vinyl]-3-(4-sulfonatobutyl)-1,3-benzothiazolium (1068434-78-5) + mercury(II) perchlorate → [(2-[(E)-2-[4-(1,4-dioxa-7,13-dithia-10-azacyclopentadec-10-yl)phenyl]vinyl]-3-(4-sulfonatobutyl)-1,3-benzothiazolium)Hg](ClO4)2 + [(2-[(E)-2-[4-(1,4-dioxa-7,13-dithia-10-azacyclopentadec-10-yl)phenyl]vinyl]-3-(4-sulfonatobutyl)-1,3-benzothiazolium)2Hg](ClO4)2

Guidance literature:

In acetonitrile; a soln. of Hg(ClO4)2 in CH3CN was added a soln. of benzothiazolium-compound in CH3CN; not sepd., detected by spectra;

DOI:10.1007/s11172-007-0082-4

upstream raw materials:

4-(1,4-dioxa-7,13-dithia-10-azacyclopentadecan-10-yl) benzaldehyde

N-(δ-sulfonatobutyl)-2-methyl-benzothiazole