C₆H₅O₂CNC₉H₆(C₂CHCHSn(CH₃)3)(O)CH(CH₃)C₂CHCHSn(CH₃)3

Base Information

Chemical Name:C₆H₅O₂CNC₉H₆(C₂CHCHSn(CH₃)3)(O)CH(CH₃)C₂CHCHSn(CH₃)3
CAS No.:650623-65-7
Molecular Formula:C₃₂H₃₇NO₃Sn₂
Molecular Weight:721.071
Hs Code.:

C<sub>6</sub>H<sub>5</sub>O<sub>2</sub>CNC<sub>9</sub>H<sub>6</sub>(C<sub>2</sub>CHCHSn(CH<sub>3</sub>)3)(O)CH(CH<sub>3</sub>)C<sub>2</sub>CHCHSn(CH<sub>3</sub>)3

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Suppliers and Price of C₆H₅O₂CNC₉H₆(C₂CHCHSn(CH₃)3)(O)CH(CH₃)C₂CHCHSn(CH₃)3

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Chemical Property of C₆H₅O₂CNC₉H₆(C₂CHCHSn(CH₃)3)(O)CH(CH₃)C₂CHCHSn(CH₃)3

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Technology Process of C₆H₅O₂CNC₉H₆(C₂CHCHSn(CH₃)3)(O)CH(CH₃)C₂CHCHSn(CH₃)3

There total 1 articles about C₆H₅O₂CNC₉H₆(C₂CHCHSn(CH₃)3)(O)CH(CH₃)C₂CHCHSn(CH₃)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

: 291743-74-3
(2S*,3S*,4R*)-3,4-epoxy-2-iodoethynyl-4-((R*)-[(3-iodo-1-methyl)prop-2-ynyl])-2H-quinoline-1-carboxylic acid phenyl ester

: 85263-63-4,98543-50-1,85271-55-2
(Z)-bis(trimethylstannyl)ethylene

: 291743-68-5
(1R*,9S*,16R*,17S*)-1,17-epoxy-16-methyl-8-phenoxycarbonyl-8-azatricyclo[7.7.1.0(2,7)]heptadeca-2⁽³⁾,4,6,12-tetraene-10.14-diyne

: 650623-65-7
C₆H₅O₂CNC₉H₆(C₂CHCHSn(CH₃)3)(O)CH(CH₃)C₂CHCHSn(CH₃)3

Guidance literature:: With lithium chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; under Ar, in the dark; bis(iodide) dissolved in DMF; Pd complex added; stirred at room temp. for 10 min; dry LiCl added; warmed to 70°C; soln. of Sn compd. in DMF added slowly over ca. 2 h; reacted for 15 min after addition; poured into crushed ice; extd. with Et2O; org. extracts washed with brine; dried (Na2SO4); filtered; solvent evapd. under reduced pressure; purified by chromy. (silica gel, petroleum ether-Et2O); elem. anal.;
DOI:10.1039/b307966j