[NBu4][(C6F5)2Pt(μ-PPh2)2Pd(acac-O,O')]

Base Information

Chemical Name:[NBu4][(C6F5)2Pt(μ-PPh2)2Pd(acac-O,O')]
CAS No.:635705-30-5
Molecular Formula:C₁₆H₃₆N*C₄₁H₂₇F₁₀O₂P₂PdPt
Molecular Weight:1347.56
Hs Code.:

Synonyms:

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Chemical Property of [NBu4][(C6F5)2Pt(μ-PPh2)2Pd(acac-O,O')]

Chemical Property:

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Technology Process of [NBu4][(C6F5)2Pt(μ-PPh2)2Pd(acac-O,O')]

There total 1 articles about [NBu4][(C6F5)2Pt(μ-PPh2)2Pd(acac-O,O')] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: (NBu4)2{(pentafluorophenyl)2platinum(II)(μ-diphenylphosphido)2palladium(II)(μ-Cl)2palladium(II)(μ-diphenylphosphido)2platinum(II)(pentafluorophenyl)2}

: thallium(I) 2,4-pentanedionate

: 55172-29-7,7791-12-0
thallium chloride

: 635705-30-5
[NBu4][(C6F5)2Pt(μ-PPh2)2Pd(acac-O,O')]

Guidance literature:: In dichloromethane; to soln. (Bu4N)2((C6F5)2Pt(μ-PPh2)2Pd(μ-Cl)2Pd(μ-PPh2)2Pt(C6F5)2) in CH2Cl2 Tl(acac) was added and stirred for 4 h; ppt. was filtered off, filtrate was concd., i-PrOH was added, ppt. was filtered off, washed with i-PrOH, and dried under vac.; elem. anal.;
DOI:10.1021/om034047f

Reference yield: 75.0%

: 73165-02-3,623171-38-0
perchlorato(triphenylphosphane)silver(I)

: 635705-30-5
[NBu4][(C6F5)2Pt(μ-PPh2)2Pd(acac-O,O')]

: [PtPdAg(μ-PPh2)2(C6F5)2(acac)(PPh3)]

Guidance literature:: In dichloromethane; to soln. (Bu4N)((C6F5)2Pt(μ-PPh2)2Pd(acac-O,O')) in CH2Cl2 (Ag(OClO3)(PPh3)) was added and stirred at room temp. for 2 h with exclusion of light; soln. was evapd. to dryness, Et2O was added, soln. was concd., hexane was added and stirred; elem. anal.;
DOI:10.1021/om034047f

Reference yield: 61.0%

: 635705-30-5
[NBu4][(C6F5)2Pt(μ-PPh2)2Pd(acac-O,O')]

: silver perchlorate

: [Pt2Pd2Ag2(μ-PPh2)4(C6F5)4(acac)2]

Guidance literature:: In dichloromethane; to soln. (Bu4N)((C6F5)2Pt(μ-PPh2)2Pd(acac)) in CH2Cl2 was added AgClO4 and stirred at room temp. for 1 h; soln. was filtered, concd., and left in freezer for 3 h, ppt. was filtered off, washed with cold CH2Cl2 and dried under vac.; elem. anal.;
DOI:10.1021/om034047f