C₁₃H₁₂ClNO₂

Base Information

• Chemical Name: C₁₃H₁₂ClNO₂
• CAS No.: 1416352-89-0
• Molecular Formula: C₁₃H₁₂ClNO₂
• Molecular Weight: 249.697
• Mol file: 1416352-89-0.mol

Synonyms:

Chemical Property of C₁₃H₁₂ClNO₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₃H₁₂ClNO₂

There total 3 articles about C₁₃H₁₂ClNO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C13H10ClNO4 → C13H12ClNO2 (1416352-89-0)

Guidance literature:

With iron; ammonium chloride; In methanol; water; at 70 ℃;

DOI:10.1016/j.bmcl.2012.10.128

Reference yield:

5-nitroguaiacol (636-93-1) → C13H12ClNO2 (1416352-89-0)

Guidance literature:

Multi-step reaction with 2 steps

1: copper diacetate; pyridine / 1,2-dichloro-ethane / 50 °C

2: iron; ammonium chloride / methanol; water / 70 °C

With pyridine; copper diacetate; iron; ammonium chloride; In methanol; water; 1,2-dichloro-ethane;

DOI:10.1016/j.bmcl.2012.10.128

Reference yield:

3-chlorophenylboronic acid (63503-60-6) → C13H12ClNO2 (1416352-89-0)

Guidance literature:

Multi-step reaction with 2 steps

1: copper diacetate; pyridine / 1,2-dichloro-ethane / 50 °C

2: iron; ammonium chloride / methanol; water / 70 °C

With pyridine; copper diacetate; iron; ammonium chloride; In methanol; water; 1,2-dichloro-ethane;

DOI:10.1016/j.bmcl.2012.10.128

upstream raw materials:

5-nitroguaiacol

3-chlorophenylboronic acid

Downstream raw materials:

C₂₂H₂₂ClN₃O₆S

C₁₃H₁₀Cl₂O₄S

C₂₃H₂₄ClN₃O₆S

Refernces