C₁₉H₃₀N₂O₂

Base Information

Chemical Name:C₁₉H₃₀N₂O₂
CAS No.:1447826-06-3
Molecular Formula:C₁₉H₃₀N₂O₂
Molecular Weight:318.459
Hs Code.:

C<sub>19</sub>H<sub>30</sub>N<sub>2</sub>O<sub>2</sub>

Synonyms:

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Chemical Property of C₁₉H₃₀N₂O₂

Chemical Property:

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Technology Process of C₁₉H₃₀N₂O₂

There total 10 articles about C₁₉H₃₀N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1447825-73-1
C₃₄H₄₀N₂O₄

: 1447826-06-3
C₁₉H₃₀N₂O₂

Guidance literature:: With potassium carbonate; In methanol; at 20 ℃; for 14h;
DOI:10.1021/jm400542h

Reference yield:

: 1447825-68-4
C₃₃H₃₉NO₄Si

: 1447826-06-3
C₁₉H₃₀N₂O₂

Guidance literature:: Multi-step reaction with 10 steps

1.1: diisobutylaluminium hydride / dichloromethane; toluene / 0.33 h / -78 °C

1.2: 1 h / 20 °C

2.1: copper(II) sulfate / dichloromethane / 22 h / 20 °C

3.1: tetrahydrofuran; dichloromethane / 0.67 h / 20 °C

4.1: hydrogenchloride / methanol; ethyl acetate / 5 h / 20 °C

5.1: sodium carbonate / tetrahydrofuran; water / 12 h / 20 °C

6.1: Dess-Martin periodane / dichloromethane / 0.5 h / 20 °C

7.1: 2-methyl-but-2-ene; sodium dihydrogenphosphate dihydrate; sodium chlorite / tetrahydrofuran; tert-butyl alcohol; water / 14 h / 20 °C

8.1: triethylamine; diphenyl phosphoryl azide / dichloromethane / 17.33 h / 0 - 20 °C

9.1: 29 h / Reflux

10.1: potassium carbonate / methanol / 14 h / 20 °C

With hydrogenchloride; sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; diphenyl phosphoryl azide; diisobutylaluminium hydride; sodium carbonate; potassium carbonate; Dess-Martin periodane; copper(II) sulfate; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; toluene; tert-butyl alcohol; 3.1: |Grignard Reaction / 6.1: |Dess-Martin Oxidation / 9.1: |Curtius Rearrangement;
DOI:10.1021/jm400542h

Reference yield:

: 1447825-71-9
C₃₅H₄₉NO₂SSi

: 1447826-06-3
C₁₉H₃₀N₂O₂

Guidance literature:: Multi-step reaction with 7 steps

1: hydrogenchloride / methanol; ethyl acetate / 5 h / 20 °C

2: sodium carbonate / tetrahydrofuran; water / 12 h / 20 °C

3: Dess-Martin periodane / dichloromethane / 0.5 h / 20 °C

4: 2-methyl-but-2-ene; sodium dihydrogenphosphate dihydrate; sodium chlorite / tetrahydrofuran; tert-butyl alcohol; water / 14 h / 20 °C

5: triethylamine; diphenyl phosphoryl azide / dichloromethane / 17.33 h / 0 - 20 °C

6: 29 h / Reflux

7: potassium carbonate / methanol / 14 h / 20 °C

With hydrogenchloride; sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; diphenyl phosphoryl azide; sodium carbonate; potassium carbonate; Dess-Martin periodane; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; tert-butyl alcohol; 3: |Dess-Martin Oxidation / 6: |Curtius Rearrangement;
DOI:10.1021/jm400542h