C₁₉H₂₃NO₂S

Base Information

Chemical Name:C₁₉H₂₃NO₂S
CAS No.:1451261-26-9
Molecular Formula:C₁₉H₂₃NO₂S
Molecular Weight:329.463
Hs Code.:

C<sub>19</sub>H<sub>23</sub>NO<sub>2</sub>S

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₉H₂₃NO₂S

Chemical Property:

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Technology Process of C₁₉H₂₃NO₂S

There total 3 articles about C₁₉H₂₃NO₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1421788-68-2
(R_S, 2S)-N-Boc-1-phenyl-3-((E)-4-phenyl-1-butenylsulfinyl)propan-2-amine

: 1451261-25-8
(3S,5R)-5-(2-phenylethyl)-3-phenylmethylthiomorpholine-1,1-dioxide

: 1451261-26-9
C₁₉H₂₃NO₂S

Guidance literature:: Multi-step reaction with 3 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / -78 - 20 °C

2.1: trifluoroacetic acid / dichloromethane / 1 h / 0 - 20 °C

2.2: pH Ca_. 8

3.1: triethylamine / methanol / 7 h / Reflux

With triethylamine; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; In methanol; dichloromethane;
DOI:10.1021/ol4023003

Reference yield:

: 1451261-09-8
(2S)-N-Boc-1-phenyl-3-((E)-4-phenyl-1-butenylsulfonyl)propan-2-amine

: 1451261-25-8
(3S,5R)-5-(2-phenylethyl)-3-phenylmethylthiomorpholine-1,1-dioxide

: 1451261-26-9
C₁₉H₂₃NO₂S

Guidance literature:: Multi-step reaction with 2 steps

1.1: trifluoroacetic acid / dichloromethane / 1 h / 0 - 20 °C

1.2: pH Ca_. 8

2.1: triethylamine / methanol / 7 h / Reflux

With triethylamine; trifluoroacetic acid; In methanol; dichloromethane;
DOI:10.1021/ol4023003

Reference yield:

: 1451261-16-7
(2S)-1-phenyl-3-((E)-4-phenyl-1-butenylsulfonyl)propan-2-amine

: 1451261-25-8
(3S,5R)-5-(2-phenylethyl)-3-phenylmethylthiomorpholine-1,1-dioxide

: 1451261-26-9
C₁₉H₂₃NO₂S

Guidance literature:: With triethylamine; In methanol; for 7h; Overall yield = 94 %; Overall yield = 90 mg; diastereoselective reaction; Reflux;
DOI:10.1021/ol4023003